[1,2,3,4,5,6]O⁶-hexakis-(toluene-4-sulfonyl)-cyclo-lin-hexa[1α=>4]-D-glucopyranosyl

Base Information

• Chemical Name: [1,2,3,4,5,6]O⁶-hexakis-(toluene-4-sulfonyl)-cyclo-lin-hexa[1α=>4]-D-glucopyranosyl
• CAS No.: 21884-25-3
• Molecular Formula: C₇₈H₉₆O₄₂S₆
• Molecular Weight: 1897.99

Synonyms:[1,2,3,4,5,6]O⁶-hexakis-(toluene-4-sulfonyl)-cyclo-lin-hexa[1α=>4]-D-glucopyranosyl

Chemical Property of [1,2,3,4,5,6]O⁶-hexakis-(toluene-4-sulfonyl)-cyclo-lin-hexa[1α=>4]-D-glucopyranosyl

Chemical Property:

Purity/Quality:

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Technology Process of [1,2,3,4,5,6]O⁶-hexakis-(toluene-4-sulfonyl)-cyclo-lin-hexa[1α=>4]-D-glucopyranosyl

There total 4 articles about [1,2,3,4,5,6]O⁶-hexakis-(toluene-4-sulfonyl)-cyclo-lin-hexa[1α=>4]-D-glucopyranosyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-toluenesulfonyl chloride (98-59-9) + alpha cyclodextrin (10016-20-3) → [1,2,3,4,5,6]O6-hexakis-(toluene-4-sulfonyl)-cyclo-lin-hexa[1α=>4]-D-glucopyranosyl (21884-25-3)

Guidance literature:

With pyridine; for 24h; Ambient temperature;

DOI:10.1021/jo00026a017

Reference yield:

p-toluenesulfonyl chloride (98-59-9) + alpha-cyclodextrin (186043-87-8) → [1,2,3,4,5,6]O6-hexakis-(toluene-4-sulfonyl)-cyclo-lin-hexa[1α=>4]-D-glucopyranosyl (21884-25-3)

Guidance literature:

With pyridine; for 3h; Ambient temperature;

DOI:10.1021/jp963916u

Reference yield:

p-toluenesulfonyl chloride (98-59-9) + alpha cyclodextrin (10016-20-3) → pentakis(6-O-tosyl)-α-CD (144872-91-3) + C85H102O44S7 (144872-92-4) + [1,2,3,4,5,6]O6-hexakis-(toluene-4-sulfonyl)-cyclo-lin-hexa[1α=>4]-D-glucopyranosyl (21884-25-3)

Guidance literature:

With bis(tri-n-butyltin)oxide; Yield given. Multistep reaction. Yields of byproduct given; 1.) toluene, reflux 2.) 50 deg C;

DOI:10.1016/S0040-4039(00)61134-6

upstream raw materials:

p-toluenesulfonyl chloride

alpha cyclodextrin

alpha-cyclodextrin

Downstream raw materials:

C₇₈H₁₀₂N₆O₂₄

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