3,6-di-O-benzyl-4-O-(2-methylnaphthyl)-β-D-mannopyranose 1,2-(ethyl orthoacetate)

Base Information

Chemical Name:3,6-di-O-benzyl-4-O-(2-methylnaphthyl)-β-D-mannopyranose 1,2-(ethyl orthoacetate)
CAS No.:1250346-33-8
Molecular Formula:C₃₅H₃₈O₇
Molecular Weight:570.683
Hs Code.:

Synonyms:3,6-di-O-benzyl-4-O-(2-methylnaphthyl)-β-D-mannopyranose 1,2-(ethyl orthoacetate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,6-di-O-benzyl-4-O-(2-methylnaphthyl)-β-D-mannopyranose 1,2-(ethyl orthoacetate)

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Technology Process of 3,6-di-O-benzyl-4-O-(2-methylnaphthyl)-β-D-mannopyranose 1,2-(ethyl orthoacetate)

There total 1 articles about 3,6-di-O-benzyl-4-O-(2-methylnaphthyl)-β-D-mannopyranose 1,2-(ethyl orthoacetate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1250346-29-2
3,6-di-O-benzyl-β-D-mannopyranose 1,2-(ethyl orthoacetate)

: 939-26-4
2-bromomethylnaphthyl bromide

: 1250346-33-8
3,6-di-O-benzyl-4-O-(2-methylnaphthyl)-β-D-mannopyranose 1,2-(ethyl orthoacetate)

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 1h;
DOI:10.1021/ol101951u

Reference yield: 62.0%

: 1250346-33-8
3,6-di-O-benzyl-4-O-(2-methylnaphthyl)-β-D-mannopyranose 1,2-(ethyl orthoacetate)

: 107-18-6
allyl alcohol

: 1250346-35-0
allyl 3,6-di-O-benzyl-4-O-(2-methylnaphthyl)-α-D-mannopyranoside

Guidance literature:: 3,6-di-O-benzyl-4-O-(2-methylnaphthyl)-β-D-mannopyranose 1,2-(ethyl orthoacetate); allyl alcohol; With trimethylsilyl trifluoromethanesulfonate; triethylamine; In dichloromethane; at 0 ℃;

With sodium methylate; In methanol; dichloromethane; at 20 ℃; for 16h;
DOI:10.1021/ol101951u