5-hydroxy-3β-acetoxy-5β-pregnanone-(20)

Base Information

• Chemical Name: 5-hydroxy-3β-acetoxy-5β-pregnanone-(20)
• CAS No.: 85220-97-9
• Molecular Formula: C₂₃H₃₆O₄
• Molecular Weight: 376.536

Synonyms:5-hydroxy-3β-acetoxy-5β-pregnanone-(20)

Chemical Property of 5-hydroxy-3β-acetoxy-5β-pregnanone-(20)

Chemical Property:

Purity/Quality:

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Technology Process of 5-hydroxy-3β-acetoxy-5β-pregnanone-(20)

There total 1 articles about 5-hydroxy-3β-acetoxy-5β-pregnanone-(20) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

pregnenolone acetate (906-83-2) → 3β-acetoxy-14α-hydroxy-5α-pregnan-20-one + 3β-acetoxy-5α-androstan-17-one (1239-31-2) + 3β-acetoxy-5α-hydroxypregnan-20-one (85220-97-9)

Guidance literature:

With tert.-butylhydroperoxide; 4 A molecular sieve; meso-5,10,15,20-tetramesitylporphyrinate osmium(II) carbonyl; In benzene; Heating;

DOI:10.1021/jo061800g

Reference yield:

5-hydroxy-3β-acetoxy-5β-pregnanone-(20) (85220-97-9) → Progesterone (57-83-0)

Guidance literature:

With potassium hydroxide; at 18 ℃; Behandeln des erhaltenen Hydrolyseprodukts mit CrO₃ in Essigsaeure und Erhitzen des Reaktionsprodukts mit Essigsaeure;

DOI:10.1002/hlca.19490320519

Reference yield:

5-hydroxy-3β-acetoxy-5β-pregnanone-(20) (85220-97-9) → Progesterone (57-83-0)

Guidance literature:

Behandeln des erhaltenen Hydrolyseprodukts mit CrO₃ in Essigsaeure und Erhitzen des Reaktionsprodukts mit Essigsaeure;

DOI:10.1002/hlca.19490320519

upstream raw materials:

pregnenolone acetate

Downstream raw materials:

Progesterone

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