C₁₀H₁₁NO

Base Information

Chemical Name:C₁₀H₁₁NO
CAS No.:71088-00-1
Molecular Formula:C₁₀H₁₁NO
Molecular Weight:161.203
Hs Code.:

Synonyms:C₁₀H₁₁NO

Suppliers and Price of C₁₀H₁₁NO

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₀H₁₁NO

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₀H₁₁NO

There total 5 articles about C₁₀H₁₁NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 68843-67-4
1-phenyl-but-3-en-1-one oxime

: 71088-00-1
C₁₀H₁₁NO

Guidance literature:: With tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; para-bromotoluene; sodium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In toluene; at 105 ℃; Inert atmosphere;
DOI:10.1021/ol8002173

Reference yield:

: 68843-67-4
(E)-1-phenylbut-3-en-1-one oxime

: 29508-04-1,71088-00-1
(1E,2E)-1-phenylbut-2-en-1-one oxime

: (1E,2Z)-1-phenylbut-2-en-1-one oxime

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; para-bromotoluene; C₂₉H₃₀NOPS; sodium t-butanolate; In toluene; at 100 ℃; for 12h; Reagent/catalyst; Overall yield = 85 percent; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.201912408

Reference yield:

: 100-52-7
benzaldehyde

: 29508-04-1,71088-00-1
(1E,2E)-1-phenylbut-2-en-1-one oxime

: (1E,2Z)-1-phenylbut-2-en-1-one oxime

Guidance literature:: Multi-step reaction with 4 steps

1: indium / tetrahydrofuran; diethyl ether / 0 °C / Inert atmosphere

2: Jones reagent / diethyl ether / 1 h / 0 - 20 °C / Inert atmosphere

3: sodium acetate; hydroxylamine hydrochloride / water; ethanol / 20 °C / Inert atmosphere

4: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium t-butanolate; para-bromotoluene; C₂₉H₃₀NOPS / toluene / 12 h / 100 °C / Inert atmosphere; Schlenk technique

With indium; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; Jones reagent; para-bromotoluene; C₂₉H₃₀NOPS; hydroxylamine hydrochloride; sodium acetate; sodium t-butanolate; In tetrahydrofuran; diethyl ether; ethanol; water; toluene;
DOI:10.1002/anie.201912408