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Technology Process of O3',O5'-hydroxyphosphoryl-1-methyl-6,N6-didehydro-1,6-dihydro-adenosine

O3',O5'-hydroxyphosphoryl-1-methyl-6,N6-didehydro-1,6-dihydro-adenosine

Base Information
  • Chemical Name:O3',O5'-hydroxyphosphoryl-1-methyl-6,N6-didehydro-1,6-dihydro-adenosine
  • CAS No.:50884-82-7
  • Molecular Formula:C11H14N5O6P
  • Molecular Weight:343.236
  • Hs Code.:
<i>O</i><sup>3'<sub>,<i>O</i></sub>5'</sup>-hydroxyphosphoryl-1-methyl-6,<i>N</i><sup>6</sup>-didehydro-1,6-dihydro-adenosine

Synonyms:O3',O5'-hydroxyphosphoryl-1-methyl-6,N6-didehydro-1,6-dihydro-adenosine

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Chemical Property of O3',O5'-hydroxyphosphoryl-1-methyl-6,N6-didehydro-1,6-dihydro-adenosine
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Technology Process of O3',O5'-hydroxyphosphoryl-1-methyl-6,N6-didehydro-1,6-dihydro-adenosine

There total 1 articles about O3',O5'-hydroxyphosphoryl-1-methyl-6,N6-didehydro-1,6-dihydro-adenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.5%

C<sub>22</sub>H<sub>38</sub>N<sub>6</sub>O<sub>6</sub>P<sup>(1+)</sup>

C22H38N6O6P(1+)

methyl iodide
74-88-4

methyl iodide

<i>O</i><sup>3'<sub>,<i>O</i></sub>5'</sup>-methoxyphosphoryl-adenosine
58937-08-9,62742-70-5,62989-52-0

O3',O5'-methoxyphosphoryl-adenosine

<i>O</i><sup>3'<sub>,<i>O</i></sub>5'</sup>-hydroxyphosphoryl-1-methyl-6,<i>N</i><sup>6</sup>-didehydro-1,6-dihydro-adenosine
50884-82-7

O3',O5'-hydroxyphosphoryl-1-methyl-6,N6-didehydro-1,6-dihydro-adenosine

cAMP
60-92-4

cAMP

Guidance literature:
With sodium carbonate; In N,N-dimethyl acetamide; at 80 ℃; for 0.0833333h; Yields of byproduct given;
DOI:10.3987/COM-91-5750
upstream raw materials:

methyl iodide

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