(+)-dimethyl-β-conidendryl alcohol

Base Information

• Chemical Name: (+)-dimethyl-β-conidendryl alcohol
• CAS No.: 66510-81-4
• Molecular Formula: C₂₂H₂₈O₆
• Molecular Weight: 388.461

Synonyms:(+)-dimethyl-β-conidendryl alcohol

Chemical Property of (+)-dimethyl-β-conidendryl alcohol

Chemical Property:

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Technology Process of (+)-dimethyl-β-conidendryl alcohol

There total 1 articles about (+)-dimethyl-β-conidendryl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

β-conidendrin dimethyl ether (25253-30-9) → (+)-dimethyl-β-conidendryl alcohol (66510-81-4)

Guidance literature:

With lithium aluminium tetrahydride; diethyl ether; benzene;

DOI:10.1021/ja01649a021

Reference yield: 70.0%

(+)-dimethyl-β-conidendryl alcohol (66510-81-4) → 2,3-bis-(hydroxymethyl)-6,7-dimethoxy-1-(3',4'-dimethoxyphenyl)naphthalene (31337-51-6) + (1R,9R,12S)-1-(3,4-Dimethoxy-phenyl)-4,5,12-trimethoxy-11-oxa-tricyclo[7.2.1.02,7]dodeca-2,4,6-triene

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 25 ℃; for 5.5h;

DOI:10.1021/jo981950u

Reference yield:

(+)-dimethyl-β-conidendryl alcohol (66510-81-4) → anhydro-β-conidendreol dimethyl ether (78215-97-1)

Guidance literature:

With potassium hydrogensulfate; at 160 ℃;

DOI:10.1021/ja01649a021

upstream raw materials:

β-conidendrin dimethyl ether

Downstream raw materials:

anhydro-β-conidendreol dimethyl ether

dimesyl-β-conidendreol dimethyl ether

ditosyl-β-conidendreol dimethyl ether

(1S,2R,3S)-1-(3,4-Dimethoxy-phenyl)-6,7-dimethoxy-2,3-bis-methoxymethyl-1,2,3,4-tetrahydro-naphthalene

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