Naphthalene, 1-(3,4-dimethoxyphenyl)-1,2,3,4-tetrahydro-6,7-dimethoxy-2,3-bis(meth oxymethyl)-, (1R,2S,3S)-rel-

Base Information

Chemical Name:Naphthalene, 1-(3,4-dimethoxyphenyl)-1,2,3,4-tetrahydro-6,7-dimethoxy-2,3-bis(meth oxymethyl)-, (1R,2S,3S)-rel-
CAS No.:50656-79-6
Molecular Formula:C₂₄H₃₂O₆
Molecular Weight:416.514
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Naphthalene, 1-(3,4-dimethoxyphenyl)-1,2,3,4-tetrahydro-6,7-dimethoxy-2,3-bis(meth oxymethyl)-, (1R,2S,3S)-rel-

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Technology Process of Naphthalene, 1-(3,4-dimethoxyphenyl)-1,2,3,4-tetrahydro-6,7-dimethoxy-2,3-bis(meth oxymethyl)-, (1R,2S,3S)-rel-

There total 20 articles about Naphthalene, 1-(3,4-dimethoxyphenyl)-1,2,3,4-tetrahydro-6,7-dimethoxy-2,3-bis(meth oxymethyl)-, (1R,2S,3S)-rel- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 63320-64-9,114839-38-2
(-)-demethylphyltetralin

: 74-88-4
methyl iodide

: 50656-79-6,63320-66-1,66428-07-7,73245-93-9,78215-55-1,123048-17-9
(+)-phyltetralin

Guidance literature:: With sodium hydride; In dimethyl sulfoxide; for 3h;
DOI:10.1021/ja00222a021

Reference yield: 83.0%

: 61248-24-6
r-1-(3,4-dimethoxyphenyl)-t-2,c-3-bis(hydroxymethyl)-6,7-dimethoxy-1,2,3,4-tetrahydronaphthalene

: 74-88-4
methyl iodide

: 50656-79-6,63320-66-1,66428-07-7,73245-93-9,78215-55-1,123048-17-9
(+/-)-phyltetralin

Guidance literature:: With sodium hydride; In dimethyl sulfoxide; for 2.5h; Ambient temperature;
DOI:10.1039/P19810001681

Reference yield:

: 54370-00-2
2-bromo-4,5-dimethoxybenzyl alcohol

: 50656-79-6,63320-66-1,66428-07-7,73245-93-9,78215-55-1,123048-17-9
(+/-)-phyltetralin

Guidance literature:: Multi-step reaction with 6 steps

3: 40percent peracetic acid

4: 90 percent / various solvent(s) / 3 h / 170 - 210 °C

5: LiAlH₄ / tetrahydrofuran

6: NaH / dimethylsulfoxide / 80 °C

With peracetic acid; lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1039/c39820000430