1-(4-acetoxyphenyl)-2-thiodihydrouracil

Base Information

Chemical Name:1-(4-acetoxyphenyl)-2-thiodihydrouracil
CAS No.:84440-08-4
Molecular Formula:C₁₂H₁₂N₂O₃S
Molecular Weight:264.305
Hs Code.:

Synonyms:1-(4-acetoxyphenyl)-2-thiodihydrouracil

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4-acetoxyphenyl)-2-thiodihydrouracil

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Technology Process of 1-(4-acetoxyphenyl)-2-thiodihydrouracil

There total 4 articles about 1-(4-acetoxyphenyl)-2-thiodihydrouracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 108-24-7
acetic anhydride

: 84439-95-2
1-(4-hydroxyphenyl)-2-thio-5,6-dihydrouracil

: 84440-08-4
1-(4-acetoxyphenyl)-2-thiodihydrouracil

Guidance literature:: With sodium hydroxide; at 3 - 5 ℃; for 20h;
DOI:10.1007/BF00503202

Reference yield:

: 123-30-8
4-amino-phenol

: 84440-08-4
1-(4-acetoxyphenyl)-2-thiodihydrouracil

Guidance literature:: Multi-step reaction with 3 steps

1: 51 percent / hydroquinone / acetic acid; propan-2-ol / 7 h / Heating

2: 81 percent / acetic acid, HCl / 120 °C / 1)AcOH,120deg C, 18h 2)conc.HCl, reflux 1h

3: 100 percent / 5percent NaOH / 20 h / 3 - 5 °C

With hydrogenchloride; sodium hydroxide; acetic acid; hydroquinone; In acetic acid; isopropyl alcohol;
DOI:10.1007/BF00503202

Reference yield:

: 70156-40-0
N-(4-hydroxyphenyl)-β-alanine methyl ester

: 84440-08-4
1-(4-acetoxyphenyl)-2-thiodihydrouracil

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / acetic acid, HCl / 120 °C / 1)AcOH,120deg C, 18h 2)conc.HCl, reflux 1h

2: 100 percent / 5percent NaOH / 20 h / 3 - 5 °C

With hydrogenchloride; sodium hydroxide; acetic acid;
DOI:10.1007/BF00503202