Sodium; 3-[3-(acetyl-benzyloxy-amino)-propylcarbamoyl]-2-{[3-(acetyl-benzyloxy-amino)-propylcarbamoyl]-methyl}-2-hydroxy-propionate

Base Information

Chemical Name:Sodium; 3-[3-(acetyl-benzyloxy-amino)-propylcarbamoyl]-2-{[3-(acetyl-benzyloxy-amino)-propylcarbamoyl]-methyl}-2-hydroxy-propionate
CAS No.:83948-78-1
Molecular Formula:C₃₀H₃₉N₄O₉*Na
Molecular Weight:622.651
Hs Code.:

Synonyms:Sodium; 3-[3-(acetyl-benzyloxy-amino)-propylcarbamoyl]-2-{[3-(acetyl-benzyloxy-amino)-propylcarbamoyl]-methyl}-2-hydroxy-propionate

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Chemical Property of Sodium; 3-[3-(acetyl-benzyloxy-amino)-propylcarbamoyl]-2-{[3-(acetyl-benzyloxy-amino)-propylcarbamoyl]-methyl}-2-hydroxy-propionate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of Sodium; 3-[3-(acetyl-benzyloxy-amino)-propylcarbamoyl]-2-{[3-(acetyl-benzyloxy-amino)-propylcarbamoyl]-methyl}-2-hydroxy-propionate

There total 16 articles about Sodium; 3-[3-(acetyl-benzyloxy-amino)-propylcarbamoyl]-2-{[3-(acetyl-benzyloxy-amino)-propylcarbamoyl]-methyl}-2-hydroxy-propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 83948-78-1
Sodium; 3-[3-(acetyl-benzyloxy-amino)-propylcarbamoyl]-2-{[3-(acetyl-benzyloxy-amino)-propylcarbamoyl]-methyl}-2-hydroxy-propionate

Guidance literature:: Multi-step reaction with 5 steps

1: 92 percent / NEt₃ / tetrahydrofuran; H₂O / 2 h / Ambient temperature

2: 41 percent / PPh₃, diisopropyl azodicarboxylate / tetrahydrofuran / 1.5 h / Ambient temperature

3: 81.7 percent / dioxane; H₂O / 50 °C

4: 1.) Et₃N / 1.) MeCN, room temperature, 1 h, 2.) 2-3 h room temperature

5: tetrahydrofuran; H₂O / 2 h

With di-isopropyl azodicarboxylate; triethylamine; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; water;
DOI:10.1021/jo00149a005

Reference yield:

: 15255-86-4
N-benzyloxycarbonyl-O-benzylhydroxylamine

: 83948-78-1
Sodium; 3-[3-(acetyl-benzyloxy-amino)-propylcarbamoyl]-2-{[3-(acetyl-benzyloxy-amino)-propylcarbamoyl]-methyl}-2-hydroxy-propionate

Guidance literature:: Multi-step reaction with 7 steps

1: 78 percent / PPh₃, DEAD / tetrahydrofuran / 1.5 h / Ambient temperature

2: 65 percent / H₂ / 5percent Pd/C / ethyl acetate / 3 h / 0 °C / 760 Torr

3: 97 percent / HCl gas / diethyl ether / 0 °C

4: Et₃N / acetonitrile / 3.5 h / Ambient temperature

5: 75 percent / dioxane; H₂O / 168 h

6: 1.) Et₃N / 1.) MeCN, room temperature, 1 h, 2.) 2-3 h room temperature

7: tetrahydrofuran; H₂O / 2 h

With hydrogenchloride; hydrogen; triethylamine; triphenylphosphine; diethylazodicarboxylate; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; diethyl ether; water; ethyl acetate; acetonitrile;
DOI:10.1021/jo00149a005

Reference yield:

: 83948-52-1
O-Benzyl-N-(p-nitrobenzyloxycarbonyl)hydroxylamine

: 83948-78-1
Sodium; 3-[3-(acetyl-benzyloxy-amino)-propylcarbamoyl]-2-{[3-(acetyl-benzyloxy-amino)-propylcarbamoyl]-methyl}-2-hydroxy-propionate

Guidance literature:: Multi-step reaction with 7 steps

1: 89 percent / PPh₃, DEAD / tetrahydrofuran / 1.5 h / Ambient temperature

2: 55 percent / H₂ / 5percent Pd/C / ethyl acetate / 3 h / 0 °C / 760 Torr

3: 97 percent / HCl gas / diethyl ether / 0 °C

4: Et₃N / acetonitrile / 3.5 h / Ambient temperature

5: 75 percent / dioxane; H₂O / 168 h

6: 1.) Et₃N / 1.) MeCN, room temperature, 1 h, 2.) 2-3 h room temperature

7: tetrahydrofuran; H₂O / 2 h

With hydrogenchloride; hydrogen; triethylamine; triphenylphosphine; diethylazodicarboxylate; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; diethyl ether; water; ethyl acetate; acetonitrile;
DOI:10.1021/jo00149a005