1-[(E)-3-(4-[1,3]dioxolan-2-yl-2-methoxy-phenyl)-allyl]-pyrrolidine-2,5-dione

Base Information

Chemical Name:1-[(E)-3-(4-[1,3]dioxolan-2-yl-2-methoxy-phenyl)-allyl]-pyrrolidine-2,5-dione
CAS No.:1443021-58-6
Molecular Formula:C₁₇H₁₉NO₅
Molecular Weight:317.342
Hs Code.:

Synonyms:1-[(E)-3-(4-[1,3]dioxolan-2-yl-2-methoxy-phenyl)-allyl]-pyrrolidine-2,5-dione

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Chemical Property of 1-[(E)-3-(4-[1,3]dioxolan-2-yl-2-methoxy-phenyl)-allyl]-pyrrolidine-2,5-dione

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Technology Process of 1-[(E)-3-(4-[1,3]dioxolan-2-yl-2-methoxy-phenyl)-allyl]-pyrrolidine-2,5-dione

There total 3 articles about 1-[(E)-3-(4-[1,3]dioxolan-2-yl-2-methoxy-phenyl)-allyl]-pyrrolidine-2,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2555-14-8
N-allylsuccinimide

: 1443021-57-5
trifluoro-methanesulfonic acid 4-[1,3]dioxolan-2-yl-2-methoxy-phenyl ester

: 1443021-58-6
1-[(E)-3-(4-[1,3]dioxolan-2-yl-2-methoxy-phenyl)-allyl]-pyrrolidine-2,5-dione

Guidance literature:: With potassium phosphate; potassium chloride; tetrabutylammomium bromide; palladium diacetate; In N,N-dimethyl-formamide; at 120 ℃; for 8h; Inert atmosphere;

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 1443021-58-6
1-[(E)-3-(4-[1,3]dioxolan-2-yl-2-methoxy-phenyl)-allyl]-pyrrolidine-2,5-dione

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / dichloromethane / 2 h / 20 °C

2: toluene-4-sulfonic acid / benzene / 180 °C

3: palladium diacetate; potassium chloride; tetrabutylammomium bromide; potassium phosphate / N,N-dimethyl-formamide / 8 h / 120 °C / Inert atmosphere

With pyridine; potassium phosphate; potassium chloride; tetrabutylammomium bromide; palladium diacetate; toluene-4-sulfonic acid; In dichloromethane; N,N-dimethyl-formamide; benzene;

Reference yield:

: 194018-68-3
vanillin triflate

: 1443021-58-6
1-[(E)-3-(4-[1,3]dioxolan-2-yl-2-methoxy-phenyl)-allyl]-pyrrolidine-2,5-dione

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / benzene / 180 °C

2: palladium diacetate; potassium chloride; tetrabutylammomium bromide; potassium phosphate / N,N-dimethyl-formamide / 8 h / 120 °C / Inert atmosphere

With potassium phosphate; potassium chloride; tetrabutylammomium bromide; palladium diacetate; toluene-4-sulfonic acid; In N,N-dimethyl-formamide; benzene;