(6-[3',6'-diaza-5'-oxo-3'-(2-triphenylmethyl thioethyl)-8'-triphenylmethylthio]octanamidohexyl β-N-acetylgalactosamine)

Base Information

Chemical Name:(6-[3',6'-diaza-5'-oxo-3'-(2-triphenylmethyl thioethyl)-8'-triphenylmethylthio]octanamidohexyl β-N-acetylgalactosamine)
CAS No.:1353721-35-3
Molecular Formula:C₆₀H₇₀N₄O₈S₂
Molecular Weight:1039.37
Hs Code.:

Synonyms:(6-[3',6'-diaza-5'-oxo-3'-(2-triphenylmethyl thioethyl)-8'-triphenylmethylthio]octanamidohexyl β-N-acetylgalactosamine)

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Chemical Property of (6-[3',6'-diaza-5'-oxo-3'-(2-triphenylmethyl thioethyl)-8'-triphenylmethylthio]octanamidohexyl β-N-acetylgalactosamine)

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Technology Process of (6-[3',6'-diaza-5'-oxo-3'-(2-triphenylmethyl thioethyl)-8'-triphenylmethylthio]octanamidohexyl β-N-acetylgalactosamine)

There total 10 articles about (6-[3',6'-diaza-5'-oxo-3'-(2-triphenylmethyl thioethyl)-8'-triphenylmethylthio]octanamidohexyl β-N-acetylgalactosamine) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1353721-33-1
(6-[3',6'-diaza-5'-oxo-3'-(2-triphenylmethylthioethyl)-8'-triphenylmethylthio]octanamidohexyl β-N-acetylgalactoseamine per-o-acetate)

: 1353721-35-3
(6-[3',6'-diaza-5'-oxo-3'-(2-triphenylmethyl thioethyl)-8'-triphenylmethylthio]octanamidohexyl β-N-acetylgalactosamine)

Guidance literature:: (6-[3',6'-diaza-5'-oxo-3'-(2"-triphenylmethylthioethyl)-8'-triphenylmethylthio]octanamidohexyl β-N-acetylgalactoseamine per-o-acetate); With sodium methylate; In methanol; at 20 ℃; for 0.5h;

With hydrogenchloride; In methanol; pH=6; Cooling with ice;

Reference yield:

: 76-84-6
triphenylmethyl alcohol

: 1353721-35-3
(6-[3',6'-diaza-5'-oxo-3'-(2-triphenylmethyl thioethyl)-8'-triphenylmethylthio]octanamidohexyl β-N-acetylgalactosamine)

Guidance literature:: Multi-step reaction with 7 steps

1.1: triethylamine / boron trifluoride diethyl etherate / chloroform / 4 h / 75 °C

2.1: triethylamine / chloroform / 2 h / 20 °C / Cooling with ice

3.1: triethylamine / dichloromethane / 48 h / Reflux

4.1: triethylamine / acetonitrile / 85 °C

5.1: potassium hydroxide / methanol / 20 °C

5.2: pH 7

6.1: triethylamine; dicyclohexyl-carbodiimide; 1-hydroxy-pyrrolidine-2,5-dione / chloroform / 48 h / Reflux

7.1: sodium methylate / methanol / 0.5 h / 20 °C

7.2: pH 6 / Cooling with ice

With 1-hydroxy-pyrrolidine-2,5-dione; sodium methylate; triethylamine; dicyclohexyl-carbodiimide; potassium hydroxide; boron trifluoride diethyl etherate; In methanol; dichloromethane; chloroform; acetonitrile;

Reference yield:

: 4048-33-3
6-amino-1-hexanol

: 1353721-35-3
(6-[3',6'-diaza-5'-oxo-3'-(2-triphenylmethyl thioethyl)-8'-triphenylmethylthio]octanamidohexyl β-N-acetylgalactosamine)

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium carbonate / diethyl ether; water / 2 h / 20 °C / Cooling with ice

2.1: mercury(II) cyanide; copper(II) sulfate / nitromethane; toluene / 24 h / 20 °C

3.1: hydrogen / palladium 10% on activated carbon / ethanol / 2585.81 Torr

4.1: triethylamine; dicyclohexyl-carbodiimide; 1-hydroxy-pyrrolidine-2,5-dione / chloroform / 48 h / Reflux

5.1: sodium methylate / methanol / 0.5 h / 20 °C

5.2: pH 6 / Cooling with ice

With 1-hydroxy-pyrrolidine-2,5-dione; hydrogen; sodium methylate; mercury(II) cyanide; sodium carbonate; copper(II) sulfate; triethylamine; dicyclohexyl-carbodiimide; palladium 10% on activated carbon; In methanol; diethyl ether; nitromethane; ethanol; chloroform; water; toluene;