(6-[3',6'-diaza-5'-oxo-3'-(2-triphenylmethylthioethyl)-8'-triphenylmethylthio]octanamidohexyl β-N-acetylgalactoseamine per-o-acetate)

Base Information

Chemical Name:(6-[3',6'-diaza-5'-oxo-3'-(2-triphenylmethylthioethyl)-8'-triphenylmethylthio]octanamidohexyl β-N-acetylgalactoseamine per-o-acetate)
CAS No.:1353721-33-1
Molecular Formula:C₆₆H₇₆N₄O₁₁S₂
Molecular Weight:1165.48
Hs Code.:

Synonyms:(6-[3',6'-diaza-5'-oxo-3'-(2-triphenylmethylthioethyl)-8'-triphenylmethylthio]octanamidohexyl β-N-acetylgalactoseamine per-o-acetate)

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Chemical Property of (6-[3',6'-diaza-5'-oxo-3'-(2-triphenylmethylthioethyl)-8'-triphenylmethylthio]octanamidohexyl β-N-acetylgalactoseamine per-o-acetate)

Chemical Property:

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Technology Process of (6-[3',6'-diaza-5'-oxo-3'-(2-triphenylmethylthioethyl)-8'-triphenylmethylthio]octanamidohexyl β-N-acetylgalactoseamine per-o-acetate)

There total 10 articles about (6-[3',6'-diaza-5'-oxo-3'-(2-triphenylmethylthioethyl)-8'-triphenylmethylthio]octanamidohexyl β-N-acetylgalactoseamine per-o-acetate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 153252-07-4
6′-aminohexyl-2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-galactoside

: 228253-42-7
3,6-diaza-5-oxo-3-[2-((triphenylmethyl)thio)ethyl]-8-[(triphenylmethyl)thio]octanoic acid

: 1353721-33-1
(6-[3',6'-diaza-5'-oxo-3'-(2-triphenylmethylthioethyl)-8'-triphenylmethylthio]octanamidohexyl β-N-acetylgalactoseamine per-o-acetate)

Guidance literature:: With 1-hydroxy-pyrrolidine-2,5-dione; triethylamine; dicyclohexyl-carbodiimide; In chloroform; for 48h; Reflux;

Reference yield:

: 76-84-6
triphenylmethyl alcohol

: 1353721-33-1
(6-[3',6'-diaza-5'-oxo-3'-(2-triphenylmethylthioethyl)-8'-triphenylmethylthio]octanamidohexyl β-N-acetylgalactoseamine per-o-acetate)

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / boron trifluoride diethyl etherate / chloroform / 4 h / 75 °C

2.1: triethylamine / chloroform / 2 h / 20 °C / Cooling with ice

3.1: triethylamine / dichloromethane / 48 h / Reflux

4.1: triethylamine / acetonitrile / 85 °C

5.1: potassium hydroxide / methanol / 20 °C

5.2: pH 7

6.1: triethylamine; dicyclohexyl-carbodiimide; 1-hydroxy-pyrrolidine-2,5-dione / chloroform / 48 h / Reflux

With 1-hydroxy-pyrrolidine-2,5-dione; triethylamine; dicyclohexyl-carbodiimide; potassium hydroxide; boron trifluoride diethyl etherate; In methanol; dichloromethane; chloroform; acetonitrile;

Reference yield:

: 4048-33-3
6-amino-1-hexanol

: 1353721-33-1
(6-[3',6'-diaza-5'-oxo-3'-(2-triphenylmethylthioethyl)-8'-triphenylmethylthio]octanamidohexyl β-N-acetylgalactoseamine per-o-acetate)

Guidance literature:: Multi-step reaction with 4 steps

1: sodium carbonate / diethyl ether; water / 2 h / 20 °C / Cooling with ice

2: mercury(II) cyanide; copper(II) sulfate / nitromethane; toluene / 24 h / 20 °C

3: hydrogen / palladium 10% on activated carbon / ethanol / 2585.81 Torr

4: triethylamine; dicyclohexyl-carbodiimide; 1-hydroxy-pyrrolidine-2,5-dione / chloroform / 48 h / Reflux

With 1-hydroxy-pyrrolidine-2,5-dione; hydrogen; mercury(II) cyanide; sodium carbonate; copper(II) sulfate; triethylamine; dicyclohexyl-carbodiimide; palladium 10% on activated carbon; In diethyl ether; nitromethane; ethanol; chloroform; water; toluene;