5-chloro-2-(triphenylphosphoranylideneamino)benzaldehyde ethylene dithioacetal

Base Information

Chemical Name:5-chloro-2-(triphenylphosphoranylideneamino)benzaldehyde ethylene dithioacetal
CAS No.:916664-17-0
Molecular Formula:C₂₇H₂₃ClNPS₂
Molecular Weight:492.045
Hs Code.:

Synonyms:5-chloro-2-(triphenylphosphoranylideneamino)benzaldehyde ethylene dithioacetal

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Chemical Property of 5-chloro-2-(triphenylphosphoranylideneamino)benzaldehyde ethylene dithioacetal

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Technology Process of 5-chloro-2-(triphenylphosphoranylideneamino)benzaldehyde ethylene dithioacetal

There total 1 articles about 5-chloro-2-(triphenylphosphoranylideneamino)benzaldehyde ethylene dithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 916664-22-7
2-azido-5-chlorobenzaldehyde ethylene dithioacetal

: 603-35-0
triphenylphosphine

: 916664-17-0
5-chloro-2-(triphenylphosphoranylideneamino)benzaldehyde ethylene dithioacetal

Guidance literature:: In diethyl ether; at 20 ℃; for 16h;
DOI:10.1021/ol062373w

Reference yield:

: 916664-17-0
5-chloro-2-(triphenylphosphoranylideneamino)benzaldehyde ethylene dithioacetal

: 525-06-4
diphenyl ketene

: (4-chloro-2-[1,3]dithiolan-2-yl-phenyl)-diphenylvinylidene-amine

Guidance literature:: In dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1021/ol062373w

Reference yield:

: 916664-17-0
5-chloro-2-(triphenylphosphoranylideneamino)benzaldehyde ethylene dithioacetal

: 6-chloro-4,4-ethylenedithio-3,3-diphenyl-3,4-dihydroquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 0.25 h / 20 °C

2: toluene / 16 h / Reflux

In toluene; 1: Aza-Wittig reaction;
DOI:10.1002/ejoc.201001372