(αS,1S,2S)-(-)-cis-2-Benzyl-N-(1-phenylethyl)cycloheptanamin-Hydrochlorid

Base Information

Chemical Name:(αS,1S,2S)-(-)-cis-2-Benzyl-N-(1-phenylethyl)cycloheptanamin-Hydrochlorid
CAS No.:135971-97-0
Molecular Formula:C₂₂H₂₉N*ClH
Molecular Weight:343.94
Hs Code.:

Synonyms:(αS,1S,2S)-(-)-cis-2-Benzyl-N-(1-phenylethyl)cycloheptanamin-Hydrochlorid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (αS,1S,2S)-(-)-cis-2-Benzyl-N-(1-phenylethyl)cycloheptanamin-Hydrochlorid

Chemical Property:

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Technology Process of (αS,1S,2S)-(-)-cis-2-Benzyl-N-(1-phenylethyl)cycloheptanamin-Hydrochlorid

There total 4 articles about (αS,1S,2S)-(-)-cis-2-Benzyl-N-(1-phenylethyl)cycloheptanamin-Hydrochlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 774-05-0
ethyl cycloheptanone-2-carboxylate

: 135971-97-0
(αS,1S,2S)-(-)-cis-2-Benzyl-N-(1-phenylethyl)cycloheptanamin-Hydrochlorid

Guidance literature:: Multi-step reaction with 3 steps

1: Na / 1.) toluene, overnight, 2.) a) room temperature, 2 h, b) reflux, 8 h

2: 70 percent / 48percent HBr / H₂O; acetic acid / Heating

3: 1.) TiCl₄, 2.) H₂ / 2.) Raney-Ni / 1.) Et₂O, pentane, reflux, 2 h, 2.) EtOH, 5 bar, 35 deg C, 10 d

With hydrogen bromide; hydrogen; sodium; titanium tetrachloride; nickel; In water; acetic acid;
DOI:10.1002/ardp.19913240604

Reference yield:

: 100-39-0
benzyl bromide

: 135971-97-0
(αS,1S,2S)-(-)-cis-2-Benzyl-N-(1-phenylethyl)cycloheptanamin-Hydrochlorid

Guidance literature:: Multi-step reaction with 3 steps

1: Na / 1.) toluene, overnight, 2.) a) room temperature, 2 h, b) reflux, 8 h

2: 70 percent / 48percent HBr / H₂O; acetic acid / Heating

3: 1.) TiCl₄, 2.) H₂ / 2.) Raney-Ni / 1.) Et₂O, pentane, reflux, 2 h, 2.) EtOH, 5 bar, 35 deg C, 10 d

With hydrogen bromide; hydrogen; sodium; titanium tetrachloride; nickel; In water; acetic acid;
DOI:10.1002/ardp.19913240604

Reference yield:

: 155854-96-9
(2-Benzylcycloheptan-1-on-2-yl)-carbonsaeureethylester

: 135971-97-0
(αS,1S,2S)-(-)-cis-2-Benzyl-N-(1-phenylethyl)cycloheptanamin-Hydrochlorid

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / 48percent HBr / H₂O; acetic acid / Heating

2: 1.) TiCl₄, 2.) H₂ / 2.) Raney-Ni / 1.) Et₂O, pentane, reflux, 2 h, 2.) EtOH, 5 bar, 35 deg C, 10 d

With hydrogen bromide; hydrogen; titanium tetrachloride; nickel; In water; acetic acid;
DOI:10.1002/ardp.19913240604