6-O-<3,4,6-tri-O-benzoyl-2-(benzoyloxyimino)-2-deoxy-β-D-arabino-hexopyranosyl>-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

Base Information

Chemical Name:6-O-<3,4,6-tri-O-benzoyl-2-(benzoyloxyimino)-2-deoxy-β-D-arabino-hexopyranosyl>-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose
CAS No.:118088-76-9
Molecular Formula:C₄₆H₄₅NO₁₅
Molecular Weight:851.861
Hs Code.:

Synonyms:6-O-<3,4,6-tri-O-benzoyl-2-(benzoyloxyimino)-2-deoxy-β-D-arabino-hexopyranosyl>-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

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Chemical Property of 6-O-<3,4,6-tri-O-benzoyl-2-(benzoyloxyimino)-2-deoxy-β-D-arabino-hexopyranosyl>-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

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Technology Process of 6-O-<3,4,6-tri-O-benzoyl-2-(benzoyloxyimino)-2-deoxy-β-D-arabino-hexopyranosyl>-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

There total 1 articles about 6-O-<3,4,6-tri-O-benzoyl-2-(benzoyloxyimino)-2-deoxy-β-D-arabino-hexopyranosyl>-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 82469-72-5
3,4,6-tri-O-benzoyl-2-(benzoyloximino)-2-deoxy-α-D-arabino-hexopyranosyl bromide

: 4064-06-6
1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

: 118088-76-9
6-O-<3,4,6-tri-O-benzoyl-2-(benzoyloxyimino)-2-deoxy-β-D-arabino-hexopyranosyl>-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

Guidance literature:: With 3 A molecular sieve; iodine; silver carbonate; In dichloromethane; for 72h; Ambient temperature; in the dark;
DOI:10.1246/bcsj.61.1291

Reference yield:

: 118088-76-9
6-O-<3,4,6-tri-O-benzoyl-2-(benzoyloxyimino)-2-deoxy-β-D-arabino-hexopyranosyl>-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

: C₃₉H₄₃NO₁₃

Guidance literature:: With diborane; In tetrahydrofuran; -10 deg C, 0.5 h; room temperature 2 h;
DOI:10.1246/bcsj.61.1291

Reference yield:

: 118088-76-9
6-O-<3,4,6-tri-O-benzoyl-2-(benzoyloxyimino)-2-deoxy-β-D-arabino-hexopyranosyl>-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

: 118088-77-0
6-O-<2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-mannopyranosyl>-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 1 M diborane / tetrahydrofuran / -10 deg C, 0.5 h; room temperature 2 h

2: 288 mg / tetrahydrofuran; methanol / 2 h / Ambient temperature

With diborane; In tetrahydrofuran; methanol;
DOI:10.1246/bcsj.61.1291