(2S,5S)-1-benzoyl-5-benzyl-5-(4'-<(benzyloxycarbonyl)amino>butyl)-2-(tert-butyl)-3-methyl-4-imidazolidinon

Base Information

Chemical Name:(2S,5S)-1-benzoyl-5-benzyl-5-(4'-<(benzyloxycarbonyl)amino>butyl)-2-(tert-butyl)-3-methyl-4-imidazolidinon
CAS No.:116139-79-8
Molecular Formula:C₃₄H₄₁N₃O₄
Molecular Weight:555.717
Hs Code.:

Synonyms:(2S,5S)-1-benzoyl-5-benzyl-5-(4'-<(benzyloxycarbonyl)amino>butyl)-2-(tert-butyl)-3-methyl-4-imidazolidinon

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Chemical Property of (2S,5S)-1-benzoyl-5-benzyl-5-(4'-<(benzyloxycarbonyl)amino>butyl)-2-(tert-butyl)-3-methyl-4-imidazolidinon

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Technology Process of (2S,5S)-1-benzoyl-5-benzyl-5-(4'-<(benzyloxycarbonyl)amino>butyl)-2-(tert-butyl)-3-methyl-4-imidazolidinon

There total 6 articles about (2S,5S)-1-benzoyl-5-benzyl-5-(4'-<(benzyloxycarbonyl)amino>butyl)-2-(tert-butyl)-3-methyl-4-imidazolidinon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 27894-50-4
methyl (2S)-2-amino-6-{[(benzyloxy)carbonyl]amino}hexanoate hydrochloride

: 116139-79-8
(2S,5S)-1-benzoyl-5-benzyl-5-(4'-<(benzyloxycarbonyl)amino>butyl)-2-(tert-butyl)-3-methyl-4-imidazolidinon

Guidance literature:: Multi-step reaction with 4 steps

1: 20.75 g / ethanol / 30 h / Ambient temperature

2: 24.2 g / CH₂Cl₂ / 16 h / Heating

3: 1.) HCl, 2.) Et₃N / 1.) MeOH, 0 deg C, 2.5 h, 2.) CH₂Cl₂, room temperature, 10 h

4: 1.) LDA / 1.) THF, -78 deg C, 30 min, 2.) THF, -78 deg C, 1 h, warm to 10 deg C for 11 h

With hydrogenchloride; triethylamine; lithium diisopropyl amide; In ethanol; dichloromethane;
DOI:10.1002/hlca.19880710124

Reference yield:

: 630-19-3
pivalaldehyde

: 116139-79-8
(2S,5S)-1-benzoyl-5-benzyl-5-(4'-<(benzyloxycarbonyl)amino>butyl)-2-(tert-butyl)-3-methyl-4-imidazolidinon

Guidance literature:: Multi-step reaction with 3 steps

1: 24.2 g / CH₂Cl₂ / 16 h / Heating

2: 1.) HCl, 2.) Et₃N / 1.) MeOH, 0 deg C, 2.5 h, 2.) CH₂Cl₂, room temperature, 10 h

3: 1.) LDA / 1.) THF, -78 deg C, 30 min, 2.) THF, -78 deg C, 1 h, warm to 10 deg C for 11 h

With hydrogenchloride; triethylamine; lithium diisopropyl amide; In dichloromethane;
DOI:10.1002/hlca.19880710124

Reference yield:

: 57499-17-9
N^ε-[(benzyloxy)carbonyl]-L-lysine N-methylamide

: 116139-79-8
(2S,5S)-1-benzoyl-5-benzyl-5-(4'-<(benzyloxycarbonyl)amino>butyl)-2-(tert-butyl)-3-methyl-4-imidazolidinon

Guidance literature:: Multi-step reaction with 3 steps

1: 24.2 g / CH₂Cl₂ / 16 h / Heating

2: 1.) HCl, 2.) Et₃N / 1.) MeOH, 0 deg C, 2.5 h, 2.) CH₂Cl₂, room temperature, 10 h

3: 1.) LDA / 1.) THF, -78 deg C, 30 min, 2.) THF, -78 deg C, 1 h, warm to 10 deg C for 11 h

With hydrogenchloride; triethylamine; lithium diisopropyl amide; In dichloromethane;
DOI:10.1002/hlca.19880710124