tert-butyl(2-methoxy-4-(methoxymethoxy)-5-vinylbenzyloxy)dimethylsilane

Base Information

Chemical Name:tert-butyl(2-methoxy-4-(methoxymethoxy)-5-vinylbenzyloxy)dimethylsilane
CAS No.:1227484-33-4
Molecular Formula:C₁₈H₃₀O₄Si
Molecular Weight:338.519
Hs Code.:

Synonyms:tert-butyl(2-methoxy-4-(methoxymethoxy)-5-vinylbenzyloxy)dimethylsilane

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Chemical Property of tert-butyl(2-methoxy-4-(methoxymethoxy)-5-vinylbenzyloxy)dimethylsilane

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Technology Process of tert-butyl(2-methoxy-4-(methoxymethoxy)-5-vinylbenzyloxy)dimethylsilane

There total 1 articles about tert-butyl(2-methoxy-4-(methoxymethoxy)-5-vinylbenzyloxy)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1227484-32-3
5-((tert-butyldimethylsilyloxy)methyl)-4-methoxy-2-(methoxymethoxy)benzaldehyde

: 1779-49-3
Methyltriphenylphosphonium bromide

: 1227484-33-4
tert-butyl(2-methoxy-4-(methoxymethoxy)-5-vinylbenzyloxy)dimethylsilane

Guidance literature:: Methyltriphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; hexane; at 20 ℃; Inert atmosphere;

5-((tert-butyldimethylsilyloxy)methyl)-4-methoxy-2-(methoxymethoxy)benzaldehyde; In tetrahydrofuran; hexane; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2010.02.089

Reference yield: 72.0%

: 1227484-33-4
tert-butyl(2-methoxy-4-(methoxymethoxy)-5-vinylbenzyloxy)dimethylsilane

: 1227484-34-5
2-(5-((tert-butyldimethylsilanyloxy)methyl)-4-methoxy-2-(methoxymethoxy)phenyl)ethanol

Guidance literature:: tert-butyl(2-methoxy-4-(methoxymethoxy)-5-vinylbenzyloxy)dimethylsilane; With dimethylsulfide borane complex; In tetrahydrofuran; diethyl ether; at 0 - 20 ℃; Inert atmosphere;

With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; diethyl ether; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tet.2010.02.089