2-[2,6-bis(hex-5-enyloxy)phenyl]-5,6,7,8-tetrahydro-8-quinolone

Base Information

• Chemical Name: 2-[2,6-bis(hex-5-enyloxy)phenyl]-5,6,7,8-tetrahydro-8-quinolone
• CAS No.: 1374423-13-8
• Molecular Formula: C₂₇H₃₃NO₃
• Molecular Weight: 419.564
• Mol file: 1374423-13-8.mol

Synonyms:2-[2,6-bis(hex-5-enyloxy)phenyl]-5,6,7,8-tetrahydro-8-quinolone

Chemical Property of 2-[2,6-bis(hex-5-enyloxy)phenyl]-5,6,7,8-tetrahydro-8-quinolone

Chemical Property:

Purity/Quality:

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Technology Process of 2-[2,6-bis(hex-5-enyloxy)phenyl]-5,6,7,8-tetrahydro-8-quinolone

There total 1 articles about 2-[2,6-bis(hex-5-enyloxy)phenyl]-5,6,7,8-tetrahydro-8-quinolone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

2-chloro-5,6,7,8-tetrahydroquinolin-8-one (129337-86-6) + [2,6-bis(hex-5-enyloxy)phenyl]boronic acid (500711-42-2) → 2-[2,6-bis(hex-5-enyloxy)phenyl]-5,6,7,8-tetrahydro-8-quinolone (1374423-13-8)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; barium hydroxide octahydrate; In 1,2-dimethoxyethane; water; for 48h; Reflux;

DOI:10.1002/ejoc.201101356

Reference yield: 48.0%

2-[2,6-bis(hex-5-enyloxy)phenyl]-5,6,7,8-tetrahydro-8-quinolone (1374423-13-8) + eschenmoser's salt (33797-51-2) → 2,12-bis[2,6-bis(hex-5-enyloxy)phenyl]-5,6,8,9-tetrahydroquino[8,7-b]-1,10-phenanthroline

Guidance literature:

With ammonium acetate; In dimethyl sulfoxide; at 85 - 130 ℃;

DOI:10.1002/ejoc.201101356

upstream raw materials:

2-chloro-5,6,7,8-tetrahydroquinolin-8-one

[2,6-bis(hex-5-enyloxy)phenyl]boronic acid