tert-butyl 2-(benzoyl)ferrocenecarboxylate

Base Information

Chemical Name:tert-butyl 2-(benzoyl)ferrocenecarboxylate
CAS No.:1004314-55-9
Molecular Formula:C₂₂H₂₂FeO₃
Molecular Weight:390.262
Hs Code.:

Synonyms:tert-butyl 2-(benzoyl)ferrocenecarboxylate

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Chemical Property of tert-butyl 2-(benzoyl)ferrocenecarboxylate

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Technology Process of tert-butyl 2-(benzoyl)ferrocenecarboxylate

There total 1 articles about tert-butyl 2-(benzoyl)ferrocenecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex

: 773156-22-2
(C₅H₅)Fe(C₅H₄CO₂C(CH₃)3)

: 98-88-4
benzoyl chloride

: 1004314-55-9
tert-butyl 2-(benzoyl)ferrocenecarboxylate

Guidance literature:: With CuCN*2LiCl; In tetrahydrofuran; 1,4-dioxane; under Ar, protected from light; Fe complex dissolved in THF-dioxane; cooled to 10°C; soln. of Mg compd. in THF added dropwise; 10°C for 2.5 h; PhCOCl and CuCN*2LiCl added at -30°C; 30 min; warmedslowly for 1-1.5 h; quenched with satd. aq. NH4Cl; monitored by GC analysis;
DOI:10.1021/om701046c