diphenylphosphorylthioformic acid piperidide

Base Information

• Chemical Name: diphenylphosphorylthioformic acid piperidide
• CAS No.: 1021879-89-9
• Molecular Formula: C₁₈H₂₀NOPS
• Molecular Weight: 329.403

Synonyms:diphenylphosphorylthioformic acid piperidide

Chemical Property of diphenylphosphorylthioformic acid piperidide

Chemical Property:

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Technology Process of diphenylphosphorylthioformic acid piperidide

There total 2 articles about diphenylphosphorylthioformic acid piperidide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

piperidine (110-89-4) + α-(diphenylphosphoryl)methyl 2-benzothiazolylsulfoxide (1028454-88-7) → diphenylphosphorylthioformic acid piperidide (1021879-89-9) + α-(diphenylphosphoryl)methyl 2-benzothiazolylsulfide (1028454-86-5) + 2-(piperidin-1-yl)benzo[d]thiazole (2851-08-3)

Guidance literature:

In 1,4-dioxane; at 90 ℃; for 1h;

DOI:10.1016/j.tet.2008.02.028

Reference yield: 30.0%

piperidine (110-89-4) + α-(diphenylphosphoryl)methyl 5-(1-phenyl)-1H-tetrazolyl sulfoxide (1021879-81-1) → phenyl-1H-tetrazole (5378-52-9) + diphenylphosphorylthioformic acid piperidide (1021879-89-9)

Guidance literature:

In 1,4-dioxane; at 90 ℃; for 1.5h;

DOI:10.1016/j.tet.2008.01.082

upstream raw materials:

piperidine

α-(diphenylphosphoryl)methyl 5-(1-phenyl)-1H-tetrazolyl sulfoxide

α-(diphenylphosphoryl)methyl 2-benzothiazolylsulfoxide

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