C₃₇H₃₈F₂O₇

Base Information

Chemical Name:C₃₇H₃₈F₂O₇
CAS No.:1181681-18-4
Molecular Formula:C₃₇H₃₈F₂O₇
Molecular Weight:632.701
Hs Code.:

C<sub>37</sub>H<sub>38</sub>F<sub>2</sub>O<sub>7</sub>

Synonyms:C₃₇H₃₈F₂O₇

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₇H₃₈F₂O₇

Chemical Property:

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Technology Process of C₃₇H₃₈F₂O₇

There total 8 articles about C₃₇H₃₈F₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1181681-15-1
C₃₇H₃₉FO₈

: 1181681-18-4
C₃₇H₃₈F₂O₇

Guidance literature:: With BAST; In tetrahydrofuran; dichloromethane; at 20 ℃; for 1h; Cooling with water;

Reference yield:

: 93777-26-5
5-bromo-2-fluorobenzaldehyde

: 1181681-18-4
C₃₇H₃₈F₂O₇

Guidance literature:: Multi-step reaction with 7 steps

1.1: n-butyllithium / toluene; tetrahydrofuran / 0.33 h / -78 °C / Inert atmosphere

1.2: 1 h / -78 °C

2.1: boron trifluoride diethyl etherate; triethylsilane / dichloromethane; acetonitrile / 0.33 h / -40 °C / Inert atmosphere

3.1: n-butyllithium / toluene; tetrahydrofuran / 0.33 h / -78 °C / Inert atmosphere

3.2: 1 h / -78 °C

4.1: boron trifluoride diethyl etherate; triethylsilane / dichloromethane; acetonitrile / 0.33 h / -40 °C / Inert atmosphere

5.1: toluene-4-sulfonic acid / dichloromethane; methanol / 1 h / 50 °C

6.1: collidine / 20 h / 20 °C

7.1: BAST / dichloromethane; tetrahydrofuran / 1 h / 20 °C / Cooling with water

With triethylsilane; n-butyllithium; boron trifluoride diethyl etherate; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; dichloromethane; toluene; acetonitrile;

Reference yield:

: 104-92-7
1-bromo-4-methoxy-benzene

: 1181681-18-4
C₃₇H₃₈F₂O₇

Guidance literature:: Multi-step reaction with 7 steps

1.1: n-butyllithium / toluene; tetrahydrofuran / 0.33 h / -78 °C / Inert atmosphere

1.2: 1 h / -78 °C

2.1: boron trifluoride diethyl etherate; triethylsilane / dichloromethane; acetonitrile / 0.33 h / -40 °C / Inert atmosphere

3.1: n-butyllithium / toluene; tetrahydrofuran / 0.33 h / -78 °C / Inert atmosphere

3.2: 1 h / -78 °C

4.1: boron trifluoride diethyl etherate; triethylsilane / dichloromethane; acetonitrile / 0.33 h / -40 °C / Inert atmosphere

5.1: toluene-4-sulfonic acid / dichloromethane; methanol / 1 h / 50 °C

6.1: collidine / 20 h / 20 °C

7.1: BAST / dichloromethane; tetrahydrofuran / 1 h / 20 °C / Cooling with water

With triethylsilane; n-butyllithium; boron trifluoride diethyl etherate; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; dichloromethane; toluene; acetonitrile;