3-phenyl-1-tri-tert-butylsilyl-1-triisopropylsilyl-1-silacyclopent-3-ene

Base Information

• Chemical Name: 3-phenyl-1-tri-tert-butylsilyl-1-triisopropylsilyl-1-silacyclopent-3-ene
• CAS No.: 366006-72-6
• Molecular Formula: C₃₁H₅₈Si₃
• Molecular Weight: 515.058
• Mol file: 366006-72-6.mol

Synonyms:3-phenyl-1-tri-tert-butylsilyl-1-triisopropylsilyl-1-silacyclopent-3-ene

Chemical Property of 3-phenyl-1-tri-tert-butylsilyl-1-triisopropylsilyl-1-silacyclopent-3-ene

Chemical Property:

Purity/Quality:

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Technology Process of 3-phenyl-1-tri-tert-butylsilyl-1-triisopropylsilyl-1-silacyclopent-3-ene

There total 1 articles about 3-phenyl-1-tri-tert-butylsilyl-1-triisopropylsilyl-1-silacyclopent-3-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-phenyl-1,3-butadiene (2288-18-8) + 2,2-dibromo-1,1,1-tri-tert-butyl-3,3,3-triisopropyltrisilane (366006-71-5) → 3-phenyl-1-tri-tert-butylsilyl-1-triisopropylsilyl-1-silacyclopent-3-ene (366006-72-6)

Guidance literature:

2-phenyl-1,3-butadiene; With magnesium; In tetrahydrofuran; at 20 ℃;

2,2-dibromo-1,1,1-tri-tert-butyl-3,3,3-triisopropyltrisilane; In tetrahydrofuran; Further stages.;

DOI:10.1021/ja016325c

Reference yield: 21.2%

3-phenyl-1-tri-tert-butylsilyl-1-triisopropylsilyl-1-silacyclopent-3-ene (366006-72-6) → chlorotriisopropylsilane (6485-79-6) + tri-t-butylsilane (18159-55-2) + 1,1,1-tri-tert-butyl-3,3,3-triisopropyltrisilane + 1,1-di-tert-butyl-4,4-dimethyl-2-triisopropylsilyl-1,2-disilatane

Guidance literature:

In various solvent(s); at 20 ℃; for 1h; under 1 Torr; Further byproducts.; Photolysis;

DOI:10.1021/ja016325c

upstream raw materials:

2-phenyl-1,3-butadiene

2,2-dibromo-1,1,1-tri-tert-butyl-3,3,3-triisopropyltrisilane

Downstream raw materials:

chlorotriisopropylsilane

tri-t-butylsilane