6-(2,4-Dichlorophenyl)-2,4-dihydroxyhexane-1-sulfonic acid

Base Information

Chemical Name:6-(2,4-Dichlorophenyl)-2,4-dihydroxyhexane-1-sulfonic acid
CAS No.:141263-69-6
Molecular Formula:C12H16 Cl2 O5 S . K
Molecular Weight:0
Hs Code.:
Mol file:141263-69-6.mol

Synonyms:6-(2,4-dichlorophenyl)-2,4-dihydroxyhexane-1-sulfonic acid;6-(2,4-dichlorophenyl)-2,4-dihydroxyhexane-1-sulfonic acid, monopotassium salt;DCPHHS

Suppliers and Price of 6-(2,4-Dichlorophenyl)-2,4-dihydroxyhexane-1-sulfonic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 6-(2,4-Dichlorophenyl)-2,4-dihydroxyhexane-1-sulfonic acid

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
PSA：103.21000
Density:g/cm³
LogP:3.00650
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:7
Exact Mass:380.9732567
Heavy Atom Count:21
Complexity:384

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C=C1Cl)Cl)CCC(CC(CS(=O)(=O)O)O)O.[K]
Isomeric SMILES:C1=CC(=C(C=C1Cl)Cl)CC[C@H](C[C@H](CS(=O)(=O)O)O)O.[K]

Technology Process of 6-(2,4-Dichlorophenyl)-2,4-dihydroxyhexane-1-sulfonic acid

There total 8 articles about 6-(2,4-Dichlorophenyl)-2,4-dihydroxyhexane-1-sulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.9%

: 141263-66-3
Diethyl 6-(2,4-dichlorophenyl)-D-erythro-2,4-isopropylidenedioxyhexylphosphonate

: 141263-69-6
Potassium 6-(2,4-dichlorophenyl)-D-erythro-2,4-dihydroxyhexane-1-sulfonate

Guidance literature:: With hydrogenchloride; In water; at 20 ℃; for 0.25h;
DOI:10.1016/S0008-6215(00)90500-7

Reference yield:

: 101910-02-5,101910-03-6,141263-55-0
(3R,5R)-5-[2-(2,4-Dichloro-phenyl)-ethyl]-tetrahydro-furan-2,3-diol

: 141263-69-6
Potassium 6-(2,4-dichlorophenyl)-D-erythro-2,4-dihydroxyhexane-1-sulfonate

Guidance literature:: Multi-step reaction with 7 steps

1: 95.6 percent / NaBH₄ / ethanol / 1 h / 0 °C

2: 78.8 percent / pyridine / 3 h / Ambient temperature

3: 89.5 percent / p-toluenesulfonic acid, 2-methoxypropene / 0.67 h / 20 °C

4: 95 percent / Bu₄NF / tetrahydrofuran / 0.67 h / 20 °C

5: 76.6 percent / triphenylphosphine, N-bromosuccinimide / CH₂Cl₂ / 0.67 h / Heating

6: 78 percent / 30 h / Heating

7: 40.9 percent / 1M HCl / H₂O / 0.25 h / 20 °C

With pyridine; hydrogenchloride; sodium tetrahydroborate; N-Bromosuccinimide; 2-Methoxypropene; tetrabutyl ammonium fluoride; toluene-4-sulfonic acid; triphenylphosphine; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1016/S0008-6215(00)90500-7

Reference yield:

: 141263-57-2
1-O-tert-Butyldimethylsilyl-6-(2,4-dichlorophenyl)-D-erythro-1,2,4-hexanetriol

: 141263-69-6
Potassium 6-(2,4-dichlorophenyl)-D-erythro-2,4-dihydroxyhexane-1-sulfonate

Guidance literature:: Multi-step reaction with 5 steps

1: 89.5 percent / p-toluenesulfonic acid, 2-methoxypropene / 0.67 h / 20 °C

2: 95 percent / Bu₄NF / tetrahydrofuran / 0.67 h / 20 °C

3: 76.6 percent / triphenylphosphine, N-bromosuccinimide / CH₂Cl₂ / 0.67 h / Heating

4: 78 percent / 30 h / Heating

5: 40.9 percent / 1M HCl / H₂O / 0.25 h / 20 °C

With hydrogenchloride; N-Bromosuccinimide; 2-Methoxypropene; tetrabutyl ammonium fluoride; toluene-4-sulfonic acid; triphenylphosphine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/S0008-6215(00)90500-7