(1R,2S,6S,7S,10S,11S)-9-Diphenylmethylene-4,4-dimethyl-3,5,8-trioxatricyclo[5.2.2.0^2,6]undecane-1,11-diol

Base Information

• Chemical Name: (1R,2S,6S,7S,10S,11S)-9-Diphenylmethylene-4,4-dimethyl-3,5,8-trioxatricyclo[5.2.2.0^2,6]undecane-1,11-diol
• CAS No.: 179677-74-8
• Molecular Formula: C₂₃H₂₄O₅
• Molecular Weight: 380.441

Synonyms:(1R,2S,6S,7S,10S,11S)-9-Diphenylmethylene-4,4-dimethyl-3,5,8-trioxatricyclo[5.2.2.0^2,6]undecane-1,11-diol

Chemical Property of (1R,2S,6S,7S,10S,11S)-9-Diphenylmethylene-4,4-dimethyl-3,5,8-trioxatricyclo[5.2.2.0^2,6]undecane-1,11-diol

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Technology Process of (1R,2S,6S,7S,10S,11S)-9-Diphenylmethylene-4,4-dimethyl-3,5,8-trioxatricyclo[5.2.2.0^2,6]undecane-1,11-diol

There total 1 articles about (1R,2S,6S,7S,10S,11S)-9-Diphenylmethylene-4,4-dimethyl-3,5,8-trioxatricyclo[5.2.2.0^2,6]undecane-1,11-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

(1R,2S,6R,7S)-9-diphenylmethylene-4,4-dimethyl-3,5,8-trioxatricyclo<5.2.2.02,6>undec-10-ene (156769-58-3) → (1R,2S,6S,7S,10S,11S)-9-Diphenylmethylene-4,4-dimethyl-3,5,8-trioxatricyclo[5.2.2.02,6]undecane-1,11-diol (179677-74-8)

Guidance literature:

With potassium carbonate; potassium hexacyanoferrate(III); osmium(VIII) oxide; In water; tert-butyl alcohol; for 20h; Ambient temperature;

DOI:10.1039/p19960001157

Reference yield: 81.0%

2,2-dimethoxy-propane (77-76-9) + (1R,2S,6S,7S,10S,11S)-9-Diphenylmethylene-4,4-dimethyl-3,5,8-trioxatricyclo[5.2.2.02,6]undecane-1,11-diol (179677-74-8) → (2R,6S,8S,12S)-14-Diphenylmethylene-4,4,10,10-tetramethyl-3,5,9,11,13-pentoxatetracyclo[5.5.2.02,6.08,12]tetradecane

Guidance literature:

With toluene-4-sulfonic acid; for 1.5h; Ambient temperature;

DOI:10.1039/p19960001157

Reference yield: 69.0%

(1R,2S,6S,7S,10S,11S)-9-Diphenylmethylene-4,4-dimethyl-3,5,8-trioxatricyclo[5.2.2.02,6]undecane-1,11-diol (179677-74-8) → 2-Hydroxy-2,2-diphenyl-1-((3aS,4R,5S,6S,7S,7aR)-5,6,7-trihydroxy-2,2-dimethyl-hexahydro-benzo[1,3]dioxol-4-yl)-ethanone

Guidance literature:

With phosphate buffer; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 2h; Ambient temperature;

DOI:10.1039/p19960001157

upstream raw materials:

(1R,2S,6R,7S)-9-diphenylmethylene-4,4-dimethyl-3,5,8-trioxatricyclo<5.2.2.0^2,6>undec-10-ene

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