Technology Process of C20H20ClF2N3O4
There total 6 articles about C20H20ClF2N3O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
2-(3-chloro-6-oxopyridin-1(6H)-yl)acetic acid; C13H16F2N2O2*(x)ClH;
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 24h;
With
hydrogenchloride;
In
water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C
2: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 24 h / 20 °C
With
hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
1,4-dioxane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / acetonitrile / 1.25 h / 50 °C
2: sodium hydroxide; methanol / tetrahydrofuran / 1.5 h / 20 °C
3: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 24 h / 20 °C
With
methanol; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide;
In
tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;