(2R,3R), 2-benzyloxycarbonylamino, 3-(4-methoxybenzylsulfanyl)-succinic acid 1-methyl ester 4-tertiobutyl ester

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Chemical Name:(2R,3R), 2-benzyloxycarbonylamino, 3-(4-methoxybenzylsulfanyl)-succinic acid 1-methyl ester 4-tertiobutyl ester
CAS No.:263552-35-8
Molecular Formula:C₂₅H₃₁NO₇S
Molecular Weight:489.59
Hs Code.:

Synonyms:(2R,3R), 2-benzyloxycarbonylamino, 3-(4-methoxybenzylsulfanyl)-succinic acid 1-methyl ester 4-tertiobutyl ester

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Chemical Property of (2R,3R), 2-benzyloxycarbonylamino, 3-(4-methoxybenzylsulfanyl)-succinic acid 1-methyl ester 4-tertiobutyl ester

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Technology Process of (2R,3R), 2-benzyloxycarbonylamino, 3-(4-methoxybenzylsulfanyl)-succinic acid 1-methyl ester 4-tertiobutyl ester

There total 2 articles about (2R,3R), 2-benzyloxycarbonylamino, 3-(4-methoxybenzylsulfanyl)-succinic acid 1-methyl ester 4-tertiobutyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 63327-57-1
(2S), 2-benzyloxycarbonylamino-succinic acid 1-methyl ester 4-tertiobutyl ester

: 191401-86-2
1-(4-methoxy-benzyldisulfanyl)-2,4-dinitrobenzene

: 263552-35-8
(2R,3R), 2-benzyloxycarbonylamino, 3-(4-methoxybenzylsulfanyl)-succinic acid 1-methyl ester 4-tertiobutyl ester

Guidance literature:: (2S), 2-benzyloxycarbonylamino-succinic acid 1-methyl ester 4-tertiobutyl ester; With n-butyllithium;

1-(4-methoxy-benzyldisulfanyl)-2,4-dinitrobenzene;
DOI:10.1021/jm9903040

Reference yield:

: 5545-52-8
Z-D(tBu)-OH

: 263552-35-8
(2R,3R), 2-benzyloxycarbonylamino, 3-(4-methoxybenzylsulfanyl)-succinic acid 1-methyl ester 4-tertiobutyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent

2: 68 percent / n-BuLi

With n-butyllithium; 1: Methylation / 2: Metallation / 2: sulfenylation;
DOI:10.1021/jm9903040

Reference yield: 68.0%

: neopentyl diethoxyphosphorylmethanesulfonate

: 263552-35-8
(2R,3R), 2-benzyloxycarbonylamino, 3-(4-methoxybenzylsulfanyl)-succinic acid 1-methyl ester 4-tertiobutyl ester

: 263552-40-5
(2R,3R), 3-benzyloxycarbonylamino-2-[4-methoxybenzylsulfanyl]-5-neopentyloxysulfonyl-pent-4-enoic acid tertiobutyl ester

Guidance literature:: neopentyl diethoxyphosphorylmethanesulfonate; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

(2R,3R), 2-benzyloxycarbonylamino, 3-(4-methoxybenzylsulfanyl)-succinic acid 1-methyl ester 4-tertiobutyl ester; With diisobutylaluminium hydride; In tetrahydrofuran; hexane; toluene; at -78 - 20 ℃; for 4h;
DOI:10.1021/jm9903040