(rac)-2-cyano-3-{6-[2-(2,6-dichloro-4-methyl-phenoxy)-ethoxy]-pyridin-3-yl}-propionic acid

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Chemical Name:(rac)-2-cyano-3-{6-[2-(2,6-dichloro-4-methyl-phenoxy)-ethoxy]-pyridin-3-yl}-propionic acid
CAS No.:948558-84-7
Molecular Formula:C₁₈H₁₆Cl₂N₂O₄
Molecular Weight:395.242
Hs Code.:

Synonyms:(rac)-2-cyano-3-{6-[2-(2,6-dichloro-4-methyl-phenoxy)-ethoxy]-pyridin-3-yl}-propionic acid

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Chemical Property of (rac)-2-cyano-3-{6-[2-(2,6-dichloro-4-methyl-phenoxy)-ethoxy]-pyridin-3-yl}-propionic acid

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Technology Process of (rac)-2-cyano-3-{6-[2-(2,6-dichloro-4-methyl-phenoxy)-ethoxy]-pyridin-3-yl}-propionic acid

There total 1 articles about (rac)-2-cyano-3-{6-[2-(2,6-dichloro-4-methyl-phenoxy)-ethoxy]-pyridin-3-yl}-propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 948558-81-4
(E)-2-cyano-3-{6-[2-(2,6-dichloro-4-methyl-phenoxy)-ethoxy]-pyridin-3-yl}-acrylic acid

: 948558-84-7
(rac)-2-cyano-3-{6-[2-(2,6-dichloro-4-methyl-phenoxy)-ethoxy]-pyridin-3-yl}-propionic acid

Guidance literature:: (E)-2-cyano-3-{6-[2-(2,6-dichloro-4-methyl-phenoxy)-ethoxy]-pyridin-3-yl}-acrylic acid; With sodium tetrahydroborate; sodium hydrogencarbonate; In methanol; water; at 0 - 20 ℃; for 5.75h;

With hydrogenchloride; In methanol; water; at 20 ℃; pH=4;

Reference yield: 67.0%

: 921630-22-0
N-({2-chloro-5-[3-(methyloxy)propyl]phenyl}methyl)cyclopropanamine

: 948558-84-7
(rac)-2-cyano-3-{6-[2-(2,6-dichloro-4-methyl-phenoxy)-ethoxy]-pyridin-3-yl}-propionic acid

: 948558-89-2
(rac)-N-[2-chloro-5-(3-methoxy-propyl)-benzyl]-2-cyano-N-cyclopropyl-3-{6-[2-(2,6-dichloro-4-methyl-phenoxy)-ethoxy]-pyridin-3-yl}-propionamide

Guidance literature:: (rac)-2-cyano-3-{6-[2-(2,6-dichloro-4-methyl-phenoxy)-ethoxy]-pyridin-3-yl}-propionic acid; With dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 0.75h;

N-({2-chloro-5-[3-(methyloxy)propyl]phenyl}methyl)cyclopropanamine; In dichloromethane; for 72h;

Reference yield: 59.0%

: 921630-23-1
N-[2-chloro-5-(2-methoxyethyl)benzyl]cyclopropanamine

: 948558-84-7
(rac)-2-cyano-3-{6-[2-(2,6-dichloro-4-methyl-phenoxy)-ethoxy]-pyridin-3-yl}-propionic acid

: 948558-88-1
(rac)-N-[2-chloro-5-(2-methoxy-ethyl)-benzyl]-2-cyano-N-cyclopropyl-3-{6-[2-(2,6-dichloro-4-methyl-phenoxy)-ethoxy]-pyridin-3-yl}-propionamide

Guidance literature:: (rac)-2-cyano-3-{6-[2-(2,6-dichloro-4-methyl-phenoxy)-ethoxy]-pyridin-3-yl}-propionic acid; With dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 0.75h;

N-[2-chloro-5-(2-methoxyethyl)benzyl]cyclopropanamine; In dichloromethane; for 72h;