C₁₉H₂₄N₂O₃

Base Information

Chemical Name:C₁₉H₂₄N₂O₃
CAS No.:75767-72-5
Molecular Formula:C₁₉H₂₄N₂O₃
Molecular Weight:328.411
Hs Code.:

C<sub>19</sub>H<sub>24</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₁₉H₂₄N₂O₃

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Chemical Property of C₁₉H₂₄N₂O₃

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Technology Process of C₁₉H₂₄N₂O₃

There total 8 articles about C₁₉H₂₄N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 75767-71-4
N-[2-((3R,3aR,7aS)-3-Methyl-6-oxo-octahydro-inden-3a-yl)-ethyl]-benzamide

: 75767-72-5
C₁₉H₂₄N₂O₃

Guidance literature:: With sodium acetate; dinitrogen tetraoxide; In dichloromethane; at -30 ℃;
DOI:10.1021/jo01314a062

Reference yield:

: 52475-64-6
ethyl-(1S,5R)-5-methyl-2-oxo-cyclopentanecarboxylate

: 75767-72-5
C₁₉H₂₄N₂O₃

Guidance literature:: Multi-step reaction with 8 steps

2: 1.) H₂; 2.) p-TsOH / Pd/C / 1.)EtOH, 1 atm, 25 deg C; 2.) toluene, reflux

3: LiAlH₄ / tetrahydrofuran / Heating

4: Et₃N / CH₂Cl₂ / 0 °C

5: 77 percent / Et₄NCl / dimethylsulfoxide / 72 h / 90 - 105 °C

6: 93 percent / LiAlH₄ / diethyl ether / 0.5 h / 25 °C

7: 80 percent / pyridine / toluene / 70 °C

8: 97 percent / N₂O₄, NaOAc / CH₂Cl₂ / -30 °C

With pyridine; lithium aluminium tetrahydride; tetraethylammonium chloride; hydrogen; sodium acetate; dinitrogen tetraoxide; toluene-4-sulfonic acid; triethylamine; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1021/jo01314a062

Reference yield:

: 75767-63-4,75767-64-5
(R)-3-Methyl-6-oxo-1,2,3,4,5,6-hexahydro-indene-3a-carboxylic acid ethyl ester

: 75767-72-5
C₁₉H₂₄N₂O₃

Guidance literature:: Multi-step reaction with 7 steps

1: 1.) H₂; 2.) p-TsOH / Pd/C / 1.)EtOH, 1 atm, 25 deg C; 2.) toluene, reflux

2: LiAlH₄ / tetrahydrofuran / Heating

3: Et₃N / CH₂Cl₂ / 0 °C

4: 77 percent / Et₄NCl / dimethylsulfoxide / 72 h / 90 - 105 °C

5: 93 percent / LiAlH₄ / diethyl ether / 0.5 h / 25 °C

6: 80 percent / pyridine / toluene / 70 °C

7: 97 percent / N₂O₄, NaOAc / CH₂Cl₂ / -30 °C

With pyridine; lithium aluminium tetrahydride; tetraethylammonium chloride; hydrogen; sodium acetate; dinitrogen tetraoxide; toluene-4-sulfonic acid; triethylamine; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1021/jo01314a062