(6S,17S)-1,4-di[N-(S)-α-phenylethyl]-1,4-diaza-6,17-diphenoxymethyl-7,10,13,19-tetraoxacyclooctadecane

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Chemical Name:(6S,17S)-1,4-di[N-(S)-α-phenylethyl]-1,4-diaza-6,17-diphenoxymethyl-7,10,13,19-tetraoxacyclooctadecane
CAS No.:1202242-77-0
Molecular Formula:C₄₂H₅₄N₂O₆
Molecular Weight:682.901
Hs Code.:

Synonyms:(6S,17S)-1,4-di[N-(S)-α-phenylethyl]-1,4-diaza-6,17-diphenoxymethyl-7,10,13,19-tetraoxacyclooctadecane

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Chemical Property of (6S,17S)-1,4-di[N-(S)-α-phenylethyl]-1,4-diaza-6,17-diphenoxymethyl-7,10,13,19-tetraoxacyclooctadecane

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Technology Process of (6S,17S)-1,4-di[N-(S)-α-phenylethyl]-1,4-diaza-6,17-diphenoxymethyl-7,10,13,19-tetraoxacyclooctadecane

There total 5 articles about (6S,17S)-1,4-di[N-(S)-α-phenylethyl]-1,4-diaza-6,17-diphenoxymethyl-7,10,13,19-tetraoxacyclooctadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 1242295-15-3
(1S,8S)-3,6-di[N-(S)-α-phenylethyl]-3,6-diaza-1,8-diphenoxymethyl-1,8-decanediol

: 19249-03-7
triethylene glycol di-(p-toluenesulfonate)

: 1202242-77-0
(6S,17S)-1,4-di[N-(S)-α-phenylethyl]-1,4-diaza-6,17-diphenoxymethyl-7,10,13,19-tetraoxacyclooctadecane

Guidance literature:: (1S,8S)-3,6-di[N-(S)-α-phenylethyl]-3,6-diaza-1,8-diphenoxymethyl-1,8-decanediol; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 3h; Inert atmosphere; Reflux;

triethylene glycol di-(p-toluenesulfonate); In tetrahydrofuran; at 0 ℃; for 50.5h; Reflux; Inert atmosphere;
DOI:10.1016/j.tetasy.2009.09.010