(1S,8S)-3,6-di[N-(S)-α-phenylethyl]-3,6-diaza-1,8-diphenoxymethyl-1,8-decanediol

Base Information

• Chemical Name: (1S,8S)-3,6-di[N-(S)-α-phenylethyl]-3,6-diaza-1,8-diphenoxymethyl-1,8-decanediol
• CAS No.: 1242295-15-3
• Molecular Formula: C₃₆H₄₄N₂O₄
• Molecular Weight: 568.756

Synonyms:(1S,8S)-3,6-di[N-(S)-α-phenylethyl]-3,6-diaza-1,8-diphenoxymethyl-1,8-decanediol

Chemical Property of (1S,8S)-3,6-di[N-(S)-α-phenylethyl]-3,6-diaza-1,8-diphenoxymethyl-1,8-decanediol

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Technology Process of (1S,8S)-3,6-di[N-(S)-α-phenylethyl]-3,6-diaza-1,8-diphenoxymethyl-1,8-decanediol

There total 2 articles about (1S,8S)-3,6-di[N-(S)-α-phenylethyl]-3,6-diaza-1,8-diphenoxymethyl-1,8-decanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.71%

(S)-1-[N-(S)-α-phenylethyl]amino-3-phenoxy-2-propanol + ethylene dibromide (106-93-4) → (1S,8S)-3,6-di[N-(S)-α-phenylethyl]-3,6-diaza-1,8-diphenoxymethyl-1,8-decanediol (1242295-15-3)

Guidance literature:

With sodium carbonate; In chloroform; at 120 ℃; for 16h; Inert atmosphere; Reflux;

DOI:10.1016/j.tetasy.2009.09.010

Reference yield: 48.71%

(S)-1-[N-(S)-α-phenylethyl]amino-3-phenoxy-2-propanol + 1,2-bis-tosyloxyethane (6315-52-2) → (1S,8S)-3,6-di[N-(S)-α-phenylethyl]-3,6-diaza-1,8-diphenoxymethyl-1,8-decanediol (1242295-15-3)

Guidance literature:

With sodium carbonate; at 120 ℃; for 12h; Inert atmosphere;

DOI:10.1080/00397910903419878

Reference yield: 94.0%

(1S,8S)-3,6-di[N-(S)-α-phenylethyl]-3,6-diaza-1,8-diphenoxymethyl-1,8-decanediol (1242295-15-3) + chloro-diphenylphosphine (1079-66-9,74391-44-9) → (1S, 8S)-3,6-[N-(S)-α-phenyl ethyl]diaza-1,8-diphenoxymethyl-1,8-octanebis(diphenylphosphinite) (1561176-84-8)

Guidance literature:

With triethylamine; In toluene; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1016/j.ica.2013.11.029

upstream raw materials:

ethylene dibromide

1,2-bis-tosyloxyethane

Downstream raw materials:

(6S,17S)-1,4-di[N-(S)-α-phenylethyl]-1,4-diaza-6,17-diphenoxymethyl-11,12-benzo-7,10,13,19-tetraoxacyclooctadec-11-ene

(6S,17S)-1,4-di[N-(S)-α-phenylethyl]-1,4-diaza-6,17-diphenoxymethyl-7,10,13,19-tetraoxacyclooctadecane

(1S, 8S)-3,6-[N-(S)-α-phenyl ethyl]diaza-1,8-diphenoxymethyl-1,8-octanebis(diphenylphosphinite)

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