C₂₅H₂₆N₈O₃

Base Information

• Chemical Name: C₂₅H₂₆N₈O₃
• CAS No.: 1596350-95-6
• Molecular Formula: C₂₅H₂₆N₈O₃
• Molecular Weight: 486.533
• Mol file: 1596350-95-6.mol

Synonyms:C₂₅H₂₆N₈O₃

Chemical Property of C₂₅H₂₆N₈O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₅H₂₆N₈O₃

There total 11 articles about C₂₅H₂₆N₈O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

C23H26N6O3 (1596350-94-5) + C3H4N2O (87718-99-8) → C25H26N8O3 (1596350-95-6)

Guidance literature:

In toluene; at 25 - 95 ℃; for 4h; Inert atmosphere;

Reference yield:

C25H29N5O3 → C25H26N8O3 (1596350-95-6)

Guidance literature:

Multi-step reaction with 3 steps

1: hydrazine hydrate; hydrazine hydro-chloride / methanol / 24 h / 75 °C / Inert atmosphere

2: acetonitrile / 20 h / 95 °C

3: toluene / 4 h / 25 - 95 °C / Inert atmosphere

With hydrazine hydrate; hydrazine hydro-chloride; In methanol; toluene; acetonitrile;

Reference yield:

C20H23N3O4 → C25H26N8O3 (1596350-95-6)

Guidance literature:

Multi-step reaction with 5 steps

1.1: sodium hydride / 1,2-dimethoxyethane / 0.33 h / 0 °C / Inert atmosphere

1.2: 2.5 h / 0 - 30 °C / Inert atmosphere

2.1: tert-Butoxybis(dimethylamino)methane / dichloromethane / 24 h / 29 °C / Inert atmosphere

3.1: hydrazine hydrate; hydrazine hydro-chloride / methanol / 24 h / 75 °C / Inert atmosphere

4.1: acetonitrile / 20 h / 95 °C

5.1: toluene / 4 h / 25 - 95 °C / Inert atmosphere

With hydrazine hydrate; tert-Butoxybis(dimethylamino)methane; hydrazine hydro-chloride; sodium hydride; In methanol; 1,2-dimethoxyethane; dichloromethane; toluene; acetonitrile;

upstream raw materials:

C₂₂H₂₄N₄O₃

C₂₃H₂₆N₆O₃

C₃H₄N₂O

(4S,5R)-ethyl-5-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)-4-meth-yl-1,3,2-dioxathiolane-4-carboxylate 2,2-dioxide