1-Phenyl-3-(trimethylsilyl)-1,2-epoxypropan

Base Information

Chemical Name:1-Phenyl-3-(trimethylsilyl)-1,2-epoxypropan
CAS No.:344417-37-4
Molecular Formula:C₁₂H₁₈OSi
Molecular Weight:206.36
Hs Code.:

Synonyms:1-Phenyl-3-(trimethylsilyl)-1,2-epoxypropan

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Phenyl-3-(trimethylsilyl)-1,2-epoxypropan

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Technology Process of 1-Phenyl-3-(trimethylsilyl)-1,2-epoxypropan

There total 4 articles about 1-Phenyl-3-(trimethylsilyl)-1,2-epoxypropan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 40595-34-4
(E)-trimethyl(3-phenylallyl)silane

: 344417-37-4
1-Phenyl-3-(trimethylsilyl)-1,2-epoxypropan

Guidance literature:: With di(chloromethyl)dioxirane; tetra(n-butyl)ammonium hydrogensulfate; edetate disodium; In acetonitrile;
DOI:10.1002/hc.10036

Reference yield: 70.0%

: 19752-23-9
cinnamyltrimethylsilane

: 344417-37-4
1-Phenyl-3-(trimethylsilyl)-1,2-epoxypropan

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1016/0022-328X(84)85135-9

Reference yield:

: 4407-36-7
(2E)-3-phenyl-2-propen-1-ol

: 344417-37-4
1-Phenyl-3-(trimethylsilyl)-1,2-epoxypropan

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N; DMAP / CH₂Cl₂ / 15 h / 0 °C

2: 73 percent / Pd(DBA)2 / tetrahydrofuran / 12 h / 20 °C

3: 97 percent / Na₂EDTA; di(chloromethyl)dioxirane; Bu₄NHSO₄ / acetonitrile

With dmap; di(chloromethyl)dioxirane; tetra(n-butyl)ammonium hydrogensulfate; edetate disodium; triethylamine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1002/hc.10036