N'-(3-ethyl-3,4,4-trimethylpentan-2-ylidene)-4-methylbenzenesulfonohydrazide

Base Information

Chemical Name:N'-(3-ethyl-3,4,4-trimethylpentan-2-ylidene)-4-methylbenzenesulfonohydrazide
CAS No.:1217009-70-5
Molecular Formula:C₁₇H₂₈N₂O₂S
Molecular Weight:324.488
Hs Code.:

Synonyms:N'-(3-ethyl-3,4,4-trimethylpentan-2-ylidene)-4-methylbenzenesulfonohydrazide

Suppliers and Price of N'-(3-ethyl-3,4,4-trimethylpentan-2-ylidene)-4-methylbenzenesulfonohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N'-(3-ethyl-3,4,4-trimethylpentan-2-ylidene)-4-methylbenzenesulfonohydrazide

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Technology Process of N'-(3-ethyl-3,4,4-trimethylpentan-2-ylidene)-4-methylbenzenesulfonohydrazide

There total 1 articles about N'-(3-ethyl-3,4,4-trimethylpentan-2-ylidene)-4-methylbenzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1217009-06-7
N'-(3,3-dichlorobutan-2-ylidene)-4-methylbenzenesulfonohydrazide

: 925-90-6
ethylmagnesium bromide

: 677-22-5
tert-butylmagnesium chloride

: 1217009-70-5
N'-(3-ethyl-3,4,4-trimethylpentan-2-ylidene)-4-methylbenzenesulfonohydrazide

Guidance literature:: ethylmagnesium bromide; With copper(l) chloride; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

N'-(3,3-dichlorobutan-2-ylidene)-4-methylbenzenesulfonohydrazide; With sodium hydride; In tetrahydrofuran; for 0.25h; Inert atmosphere; Cooling;

tert-butylmagnesium chloride; Further stages;
DOI:10.1021/ja100932q