1-((1S,2S)-2-methoxyindan-1-yl)-3-pentamethylphenylimidazoliniumHexafluorophosphate

Base Information

Chemical Name:1-((1S,2S)-2-methoxyindan-1-yl)-3-pentamethylphenylimidazoliniumHexafluorophosphate
CAS No.:1579250-28-4
Molecular Formula:C₂₄H₃₁N₂O*F₆P
Molecular Weight:508.487
Hs Code.:

Synonyms:1-((1S,2S)-2-methoxyindan-1-yl)-3-pentamethylphenylimidazoliniumHexafluorophosphate

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Chemical Property of 1-((1S,2S)-2-methoxyindan-1-yl)-3-pentamethylphenylimidazoliniumHexafluorophosphate

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Technology Process of 1-((1S,2S)-2-methoxyindan-1-yl)-3-pentamethylphenylimidazoliniumHexafluorophosphate

There total 5 articles about 1-((1S,2S)-2-methoxyindan-1-yl)-3-pentamethylphenylimidazoliniumHexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1579250-24-0
1-((1S,2S)-2-hydroxyindan-1-yl)-3-pentamethylphenylimidazolinium hexafluorophosphate

: 18107-18-1
diazomethyl-trimethyl-silane

: 1579250-28-4
1-((1S,2S)-2-methoxyindan-1-yl)-3-pentamethylphenylimidazoliniumHexafluorophosphate

Guidance literature:: 1-((1S,2S)-2-hydroxyindan-1-yl)-3-pentamethylphenylimidazolinium hexafluorophosphate; diazomethyl-trimethyl-silane; With tetrafluoroboric acid; In diethyl ether; dichloromethane; water; at 0 ℃; for 0.25h;

With potassium hexafluorophosphate; In methanol; water; at 20 ℃; for 1h;
DOI:10.1021/jo500068p

Reference yield:

: 2243-30-3,738542-25-1
pentamethylaniline

: 1579250-28-4
1-((1S,2S)-2-methoxyindan-1-yl)-3-pentamethylphenylimidazoliniumHexafluorophosphate

Guidance literature:: Multi-step reaction with 5 steps

1.1: pyridine / dichloromethane / 18 h / 0 - 20 °C

2.1: dichloromethane / 60 h / Reflux

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 16 h / 0 - 70 °C

4.1: hydrogenchloride / diethyl ether / 0.25 h / 20 °C

4.2: 19 h / 90 °C

4.3: 2 h / 20 °C

5.1: tetrafluoroboric acid / dichloromethane; diethyl ether; water / 0.25 h / 0 °C

5.2: 1 h / 20 °C

With pyridine; hydrogenchloride; lithium aluminium tetrahydride; tetrafluoroboric acid; In tetrahydrofuran; diethyl ether; dichloromethane; water;
DOI:10.1021/jo500068p

Reference yield:

: 1579250-33-1
N-(2,3,4,5,6-pentamethylphenyl)-N′-((1S,2S)-2-hydroxy-1-indanyl)oxalamide

: 1579250-28-4
1-((1S,2S)-2-methoxyindan-1-yl)-3-pentamethylphenylimidazoliniumHexafluorophosphate

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 16 h / 0 - 70 °C

2.1: hydrogenchloride / diethyl ether / 0.25 h / 20 °C

2.2: 19 h / 90 °C

2.3: 2 h / 20 °C

3.1: tetrafluoroboric acid / dichloromethane; diethyl ether; water / 0.25 h / 0 °C

3.2: 1 h / 20 °C

With hydrogenchloride; lithium aluminium tetrahydride; tetrafluoroboric acid; In tetrahydrofuran; diethyl ether; dichloromethane; water;
DOI:10.1021/jo500068p