1-((1S,2S)-2-hydroxyindan-1-yl)-3-pentamethylphenylimidazolinium hexafluorophosphate

Base Information

Chemical Name:1-((1S,2S)-2-hydroxyindan-1-yl)-3-pentamethylphenylimidazolinium hexafluorophosphate
CAS No.:1579250-24-0
Molecular Formula:C₂₃H₂₉N₂O*F₆P
Molecular Weight:494.46
Hs Code.:

Synonyms:1-((1S,2S)-2-hydroxyindan-1-yl)-3-pentamethylphenylimidazolinium hexafluorophosphate

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Chemical Property of 1-((1S,2S)-2-hydroxyindan-1-yl)-3-pentamethylphenylimidazolinium hexafluorophosphate

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Technology Process of 1-((1S,2S)-2-hydroxyindan-1-yl)-3-pentamethylphenylimidazolinium hexafluorophosphate

There total 4 articles about 1-((1S,2S)-2-hydroxyindan-1-yl)-3-pentamethylphenylimidazolinium hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₂H₃₀N₂O

: 149-73-5
trimethyl orthoformate

: 1579250-24-0
1-((1S,2S)-2-hydroxyindan-1-yl)-3-pentamethylphenylimidazolinium hexafluorophosphate

Guidance literature:: C₂₂H₃₀N₂O; With hydrogenchloride; In diethyl ether; at 20 ℃; for 0.25h;

trimethyl orthoformate; In toluene; at 90 ℃; for 19h;

With potassium hexafluorophosphate; In methanol; water; at 20 ℃; for 2h;
DOI:10.1021/jo500068p

Reference yield:

: 2243-30-3,738542-25-1
pentamethylaniline

: 1579250-24-0
1-((1S,2S)-2-hydroxyindan-1-yl)-3-pentamethylphenylimidazolinium hexafluorophosphate

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine / dichloromethane / 18 h / 0 - 20 °C

2.1: dichloromethane / 60 h / Reflux

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 16 h / 0 - 70 °C

4.1: hydrogenchloride / diethyl ether / 0.25 h / 20 °C

4.2: 19 h / 90 °C

4.3: 2 h / 20 °C

With pyridine; hydrogenchloride; lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/jo500068p

Reference yield:

: 1579250-33-1
N-(2,3,4,5,6-pentamethylphenyl)-N′-((1S,2S)-2-hydroxy-1-indanyl)oxalamide

: 1579250-24-0
1-((1S,2S)-2-hydroxyindan-1-yl)-3-pentamethylphenylimidazolinium hexafluorophosphate

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 16 h / 0 - 70 °C

2.1: hydrogenchloride / diethyl ether / 0.25 h / 20 °C

2.2: 19 h / 90 °C

2.3: 2 h / 20 °C

With hydrogenchloride; lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jo500068p