N-<3-(2,3-dibenzyloxybenzoylamino)propyl>-N-<4-(2,3-dibenzyloxybenzoylamino)butyl>-2-benzyloxybenzoylalanylamide

Base Information

Chemical Name:N-<3-(2,3-dibenzyloxybenzoylamino)propyl>-N-<4-(2,3-dibenzyloxybenzoylamino)butyl>-2-benzyloxybenzoylalanylamide
CAS No.:161219-96-1
Molecular Formula:C₆₆H₆₆N₄O₉
Molecular Weight:1059.27
Hs Code.:

Synonyms:N-<3-(2,3-dibenzyloxybenzoylamino)propyl>-N-<4-(2,3-dibenzyloxybenzoylamino)butyl>-2-benzyloxybenzoylalanylamide

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Chemical Property of N-<3-(2,3-dibenzyloxybenzoylamino)propyl>-N-<4-(2,3-dibenzyloxybenzoylamino)butyl>-2-benzyloxybenzoylalanylamide

Chemical Property:

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Technology Process of N-<3-(2,3-dibenzyloxybenzoylamino)propyl>-N-<4-(2,3-dibenzyloxybenzoylamino)butyl>-2-benzyloxybenzoylalanylamide

There total 3 articles about N-<3-(2,3-dibenzyloxybenzoylamino)propyl>-N-<4-(2,3-dibenzyloxybenzoylamino)butyl>-2-benzyloxybenzoylalanylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4349-62-6
2-benzyloxybenzoyl chloride

: 161219-96-1
N-<3-(2,3-dibenzyloxybenzoylamino)propyl>-N-<4-(2,3-dibenzyloxybenzoylamino)butyl>-2-benzyloxybenzoylalanylamide

Guidance literature:: Multi-step reaction with 3 steps

2: aq. sodium hydroxide

3: 1.) diphenylphosphoryl azide; 2.) triethylamine, dimethylaminopyridine / dimethylformamide / 1.) 0 deg C; 2.) rt., 2 d

With dmap; sodium hydroxide; diphenylphosphoranyl azide; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)85669-6

Reference yield:

: 68939-34-4
N-(o-Benzyloxy-benzoyl)-L-alanin-methylester

: 161219-96-1
N-<3-(2,3-dibenzyloxybenzoylamino)propyl>-N-<4-(2,3-dibenzyloxybenzoylamino)butyl>-2-benzyloxybenzoylalanylamide

Guidance literature:: Multi-step reaction with 2 steps

1: aq. sodium hydroxide

2: 1.) diphenylphosphoryl azide; 2.) triethylamine, dimethylaminopyridine / dimethylformamide / 1.) 0 deg C; 2.) rt., 2 d

With dmap; sodium hydroxide; diphenylphosphoranyl azide; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)85669-6

Reference yield:

: 68939-46-8
N-(o-Benzyloxy-benzoyl)-L-alanin

: 74272-81-4
2,3-bis(benzyloxy)-N-(3-(4-(2,3-bis(benzyloxy)benzamido)butylamino)propyl)benzamide

: 161219-96-1
N-<3-(2,3-dibenzyloxybenzoylamino)propyl>-N-<4-(2,3-dibenzyloxybenzoylamino)butyl>-2-benzyloxybenzoylalanylamide

Guidance literature:: With dmap; diphenylphosphoranyl azide; triethylamine; In N,N-dimethyl-formamide; 1.) 0 deg C; 2.) rt., 2 d;
DOI:10.1016/S0040-4020(01)85669-6