N-[N'-(diphenylmethylene)-(S)-p-(2-ethyl-1,3-dioxolan-2-yl)-phenylalanyl]-(-)-10,2-bornane sultam

Base Information

Chemical Name:N-[N'-(diphenylmethylene)-(S)-p-(2-ethyl-1,3-dioxolan-2-yl)-phenylalanyl]-(-)-10,2-bornane sultam
CAS No.:449141-99-5
Molecular Formula:C₃₇H₄₂N₂O₅S
Molecular Weight:626.817
Hs Code.:

Synonyms:N-[N'-(diphenylmethylene)-(S)-p-(2-ethyl-1,3-dioxolan-2-yl)-phenylalanyl]-(-)-10,2-bornane sultam

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Chemical Property of N-[N'-(diphenylmethylene)-(S)-p-(2-ethyl-1,3-dioxolan-2-yl)-phenylalanyl]-(-)-10,2-bornane sultam

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Technology Process of N-[N'-(diphenylmethylene)-(S)-p-(2-ethyl-1,3-dioxolan-2-yl)-phenylalanyl]-(-)-10,2-bornane sultam

There total 4 articles about N-[N'-(diphenylmethylene)-(S)-p-(2-ethyl-1,3-dioxolan-2-yl)-phenylalanyl]-(-)-10,2-bornane sultam which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 138566-17-3
2-(benzhydrylideneamino)-1-(10,10-dimethyl-3,3-dioxo-3λ⁶-thia-4-aza-tricyclo[5.2.1.0^1.5]dec-4-yl)ethanone

: 449141-98-4
2-(p-bromomethyl-phenyl)-2-ethyl-1,3-dioxolane

: 449141-99-5
N-[N'-(diphenylmethylene)-(S)-p-(2-ethyl-1,3-dioxolan-2-yl)-phenylalanyl]-(-)-10,2-bornane sultam

Guidance literature:: 2-(benzhydrylideneamino)-1-(10,10-dimethyl-3,3-dioxo-3λ⁶-thia-4-aza-tricyclo[5.2.1.0^1.5]dec-4-yl)ethanone; With lithium diisopropyl amide; In tetrahydrofuran; n-heptane; at -78 ℃; for 0.25h;

2-(p-bromomethyl-phenyl)-2-ethyl-1,3-dioxolane; In tetrahydrofuran; n-heptane; at -78 - 20 ℃; for 2h;
DOI:10.1002/1099-0690(200205)2002:10<1677::AID-EJOC1677>3.0.CO;2-8

Reference yield:

: 5337-93-9
4'-methylpropiophenone

: 449141-99-5
N-[N'-(diphenylmethylene)-(S)-p-(2-ethyl-1,3-dioxolan-2-yl)-phenylalanyl]-(-)-10,2-bornane sultam

Guidance literature:: Multi-step reaction with 3 steps

1.1: 86 percent / PTSA / toluene / 24 h / Heating

2.1: 47 percent / NBS; benzoyl peroxide / cyclohexane / 4 h / Heating

3.1: LDA / tetrahydrofuran; heptane; various solvent(s) / 0.25 h / -78 °C

3.2: 54 percent / tetrahydrofuran; heptane; various solvent(s) / 2 h / -78 - 20 °C

With N-Bromosuccinimide; toluene-4-sulfonic acid; lithium diisopropyl amide; dibenzoyl peroxide; In tetrahydrofuran; n-heptane; cyclohexane; toluene;
DOI:10.1002/1099-0690(200205)2002:10<1677::AID-EJOC1677>3.0.CO;2-8

Reference yield:

: 91306-50-2
α-phenylselenenyl-4'-methylpropiophenone

: 449141-99-5
N-[N'-(diphenylmethylene)-(S)-p-(2-ethyl-1,3-dioxolan-2-yl)-phenylalanyl]-(-)-10,2-bornane sultam

Guidance literature:: Multi-step reaction with 4 steps

1.1: HF; dimethylsulfide; anisole / tetrahydrofuran

2.1: 86 percent / PTSA / toluene / 24 h / Heating

3.1: 47 percent / NBS; benzoyl peroxide / cyclohexane / 4 h / Heating

4.1: LDA / tetrahydrofuran; heptane; various solvent(s) / 0.25 h / -78 °C

4.2: 54 percent / tetrahydrofuran; heptane; various solvent(s) / 2 h / -78 - 20 °C

With N-Bromosuccinimide; dimethylsulfide; hydrogen fluoride; toluene-4-sulfonic acid; methoxybenzene; lithium diisopropyl amide; dibenzoyl peroxide; In tetrahydrofuran; n-heptane; cyclohexane; toluene;
DOI:10.1002/1099-0690(200205)2002:10<1677::AID-EJOC1677>3.0.CO;2-8