6-O-benzoyl-3-deoxy-1,2-O-isopropylidene-5-O-tosyl-α-D-xylo-hexofuranose

Base Information

Chemical Name:6-O-benzoyl-3-deoxy-1,2-O-isopropylidene-5-O-tosyl-α-D-xylo-hexofuranose
CAS No.:457073-50-6
Molecular Formula:C₂₃H₂₆O₈S
Molecular Weight:462.521
Hs Code.:

Synonyms:6-O-benzoyl-3-deoxy-1,2-O-isopropylidene-5-O-tosyl-α-D-xylo-hexofuranose

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Chemical Property of 6-O-benzoyl-3-deoxy-1,2-O-isopropylidene-5-O-tosyl-α-D-xylo-hexofuranose

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Technology Process of 6-O-benzoyl-3-deoxy-1,2-O-isopropylidene-5-O-tosyl-α-D-xylo-hexofuranose

There total 4 articles about 6-O-benzoyl-3-deoxy-1,2-O-isopropylidene-5-O-tosyl-α-D-xylo-hexofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 98-59-9
p-toluenesulfonyl chloride

: 457073-51-7
6-O-benzoyl-3-deoxy-1,2-O-isopropylidene-α-D-xylo-hexofuranose

: 457073-50-6
6-O-benzoyl-3-deoxy-1,2-O-isopropylidene-5-O-tosyl-α-D-xylo-hexofuranose

Guidance literature:: With pyridine; at 20 ℃; for 12h;
DOI:10.1135/cccc20020622

Reference yield: 90.0%

: 532-32-1
sodium benzoate

: 75646-88-7
3-deoxy-1,2-O-isopropylidene-5,6-di-O-tosyl-α-D-xylo-hexofuranose

: 457073-50-6
6-O-benzoyl-3-deoxy-1,2-O-isopropylidene-5-O-tosyl-α-D-xylo-hexofuranose

Guidance literature:: In N,N-dimethyl-formamide; at 80 ℃; for 6h;
DOI:10.1135/cccc20020622

Reference yield:

: 4005-46-3
(1R)-1-[(3aR,5R,6aR)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl]ethane-1,2-diol

: 457073-50-6
6-O-benzoyl-3-deoxy-1,2-O-isopropylidene-5-O-tosyl-α-D-xylo-hexofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 46 percent / pyridine / CHCl₃ / 12 h / 20 °C

2: 94 percent / pyridine / 12 h / 20 °C

With pyridine; In chloroform;
DOI:10.1135/cccc20020622