C₂₃H₁₅F₃O₂S

Base Information

Chemical Name:C₂₃H₁₅F₃O₂S
CAS No.:1613391-10-8
Molecular Formula:C₂₃H₁₅F₃O₂S
Molecular Weight:412.432
Hs Code.:

C<sub>23</sub>H<sub>15</sub>F<sub>3</sub>O<sub>2</sub>S

Synonyms:C₂₃H₁₅F₃O₂S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₃H₁₅F₃O₂S

Chemical Property:

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Technology Process of C₂₃H₁₅F₃O₂S

There total 6 articles about C₂₃H₁₅F₃O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1207970-84-0
ethyl 3-{2-[3-(trifluoromethyl)benzyl]-1-benzothiophen-7-yl}benzoate

: 1613391-10-8
C₂₃H₁₅F₃O₂S

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; methanol; ethanol; at 60 ℃; for 0.5h;
DOI:10.1021/jm5002919

Reference yield:

: 1171926-64-9
(7-bromo-1-benzothiophen-2-yl)methanol

: 1613391-10-8
C₂₃H₁₅F₃O₂S

Guidance literature:: Multi-step reaction with 4 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,2-dimethoxyethane; water / 16 h / Reflux; Inert atmosphere

2: phosphorus tribromide / diethyl ether / 2 h / 20 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,2-dimethoxyethane; water / 14 h / 85 °C / Inert atmosphere

4: sodium hydroxide / methanol; ethanol; tetrahydrofuran / 0.5 h / 60 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; phosphorus tribromide; sodium carbonate; sodium hydroxide; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; diethyl ether; ethanol; water; 1: |Suzuki Coupling / 3: |Suzuki Coupling;
DOI:10.1021/jm5002919

Reference yield:

: 1207970-52-2
ethyl 3-[2-(Hydroxymethyl)-1-benzothiophen-7-yl]benzoate

: 1613391-10-8
C₂₃H₁₅F₃O₂S

Guidance literature:: Multi-step reaction with 3 steps

1: phosphorus tribromide / diethyl ether / 2 h / 20 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,2-dimethoxyethane; water / 14 h / 85 °C / Inert atmosphere

3: sodium hydroxide / methanol; ethanol; tetrahydrofuran / 0.5 h / 60 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; phosphorus tribromide; sodium carbonate; sodium hydroxide; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; diethyl ether; ethanol; water; 2: |Suzuki Coupling;
DOI:10.1021/jm5002919