2-[2-(3,4-dimethoxyphenyl)ethyl]-1-methyl-1,2,3,4-tetrahydroquinolineanol

Base Information

Chemical Name:2-[2-(3,4-dimethoxyphenyl)ethyl]-1-methyl-1,2,3,4-tetrahydroquinolineanol
CAS No.:104967-55-7
Molecular Formula:C₂₀H₂₅NO₂
Molecular Weight:311.424
Hs Code.:

Synonyms:2-[2-(3,4-dimethoxyphenyl)ethyl]-1-methyl-1,2,3,4-tetrahydroquinolineanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[2-(3,4-dimethoxyphenyl)ethyl]-1-methyl-1,2,3,4-tetrahydroquinolineanol

Chemical Property:

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Technology Process of 2-[2-(3,4-dimethoxyphenyl)ethyl]-1-methyl-1,2,3,4-tetrahydroquinolineanol

There total 25 articles about 2-[2-(3,4-dimethoxyphenyl)ethyl]-1-methyl-1,2,3,4-tetrahydroquinolineanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: N-methyl-2-(3,4-dimethoxyphenylethynyl)-1,2,3,4-tetrahydroquinoline

: 104967-55-7,442-33-1
2-[2-(3,4-dimethoxyphenyl)ethyl]-1-methyl-1,2,3,4-tetrahydroquinolineanol

Guidance literature:: With 5%-palladium/activated carbon; hydrogen; In methanol; at 20 ℃;

Reference yield: 95.0%

: 104967-54-6
2-(3,4-dimethoxy-β-phenethyl)-1,2,3,4-tetrahydroquinoline

: 74-88-4
methyl iodide

: 104967-55-7,442-33-1
2-[2-(3,4-dimethoxyphenyl)ethyl]-1-methyl-1,2,3,4-tetrahydroquinolineanol

Guidance literature:: With potassium carbonate; In tetrahydrofuran; for 20h; Reflux;
DOI:10.1039/c9ob02673h

Reference yield: 77.0%

: 77669-22-8
2-(3,4-dimethoxyphenylethenyl)quinoline

: 74-88-4
methyl iodide

: 104967-55-7,442-33-1
2-[2-(3,4-dimethoxyphenyl)ethyl]-1-methyl-1,2,3,4-tetrahydroquinolineanol

Guidance literature:: 2-(3,4-dimethoxyphenylethenyl)quinoline; With methanol; sodium tetrahydroborate; nickel(II) chloride hexahydrate; at 0 - 20 ℃; for 0.5h;

methyl iodide; With potassium carbonate; In tetrahydrofuran; for 20h; Sealed tube; Reflux;
DOI:10.1021/acs.orglett.0c04060