2-AMino-3-carbaMoyl-4,7-dihydro-5H-thieno[2,3-c]pyridine-6-carboxylic acid benzyl ester

Base Information

• Chemical Name: 2-AMino-3-carbaMoyl-4,7-dihydro-5H-thieno[2,3-c]pyridine-6-carboxylic acid benzyl ester
• CAS No.: 869278-52-4
• Molecular Formula: C₁₆H₁₇N₃O₃S
• Molecular Weight: 331.395
• Mol file: 869278-52-4.mol

Synonyms:benzyl 2-amino-3-carbamoyl-4,5-dihydrothieno[2,3-c]pyridine-6(7H)-carboxylate

Chemical Property of 2-AMino-3-carbaMoyl-4,7-dihydro-5H-thieno[2,3-c]pyridine-6-carboxylic acid benzyl ester

Chemical Property:

• Storage Temp.: 2-8°C

Purity/Quality:

98% ^*data from raw suppliers

Benzyl2-amino-3-carbamoyl-4,5-dihydrothieno[2,3-c]pyridine-6(7H)-carboxylate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of 2-AMino-3-carbaMoyl-4,7-dihydro-5H-thieno[2,3-c]pyridine-6-carboxylic acid benzyl ester

There total 1 articles about 2-AMino-3-carbaMoyl-4,7-dihydro-5H-thieno[2,3-c]pyridine-6-carboxylic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl 4-oxo-1-piperidinecarboxylate (19099-93-5) + cyanoacetic acid amide (107-91-5) → benzyl 2-amino-3-carbamoyl-4,5-dihydrothieno[2,3-c]pyridine-6(7H)-carboxylate (869278-52-4)

Guidance literature:

With morpholine; sulfur; In ethanol; at 60 ℃; for 1h;

DOI:10.1016/j.bmcl.2005.07.072

Reference yield: 58.0%

benzyl 2-amino-3-carbamoyl-4,5-dihydrothieno[2,3-c]pyridine-6(7H)-carboxylate (869278-52-4) + 3,4-dimethoxy-5-iodobenzaldehyde (32024-15-0) → 2-(3-iodo-4,5-dimethoxyphenyl)-7-benzoxycarbonyl-5,6,7,8-tetrahydropyridylthieno[2,3-d]pyrimidin-4(3H)-one

Guidance literature:

With hydrogenchloride; In butan-1-ol; at 80 ℃; for 1h;

DOI:10.1016/j.ejmech.2020.112060

Reference yield: 50.0%

benzyl 2-amino-3-carbamoyl-4,5-dihydrothieno[2,3-c]pyridine-6(7H)-carboxylate (869278-52-4) + 5-chloroveratraldehyde (18268-68-3) → 2-(3-chloro-4,5-dimethoxyphenyl)-7-benzoxycarbonyl-5,6,7,8-tetrahydropyridylthieno[2,3-d]pyrimidin-4(3H)-one

Guidance literature:

With hydrogenchloride; In butan-1-ol; at 80 ℃; for 1h;

DOI:10.1016/j.ejmech.2020.112060

upstream raw materials:

benzyl 4-oxo-1-piperidinecarboxylate

cyanoacetic acid amide

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