Technology Process of C25H25N3S
There total 6 articles about C25H25N3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
ethanol;
at 80 ℃;
for 0.333333h;
Sealed vessel;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: acetic acid / 24 h / 90 °C
2.1: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere; Reflux
3.1: trifluoroacetic acid / ethanol / 3 h / Reflux
3.2: 2 h / Reflux
4.1: toluene; benzene / 0.17 h / 0 °C
4.2: 4 h / 20 °C
5.1: triethylamine; hydrogen sulfide / pyridine / 72 h / 20 °C
6.1: hydrogenchloride / ethanol / 0.33 h / 80 °C / Sealed vessel
With
hydrogenchloride; lithium aluminium tetrahydride; hydrogen sulfide; acetic acid; triethylamine; trifluoroacetic acid;
In
tetrahydrofuran; pyridine; ethanol; toluene; benzene;
3.1: Pictet-Spengler Cyclisation / 3.2: Pictet-Spengler Cyclisation;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine; hydrogen sulfide / pyridine / 72 h / 20 °C
2: hydrogenchloride / ethanol / 0.33 h / 80 °C / Sealed vessel
With
hydrogenchloride; hydrogen sulfide; triethylamine;
In
pyridine; ethanol;