N,N'-bis(4-chlorophenyl)-1,7-(disulfuric acid)perylene-3,4,9,10-tetracarboxy diimide

Base Information

• Chemical Name: N,N'-bis(4-chlorophenyl)-1,7-(disulfuric acid)perylene-3,4,9,10-tetracarboxy diimide
• CAS No.: 1200827-15-1
• Molecular Formula: C₃₆H₁₆Cl₂N₂O₁₀S₂
• Molecular Weight: 771.568
• Mol file: 1200827-15-1.mol

Synonyms:N,N'-bis(4-chlorophenyl)-1,7-(disulfuric acid)perylene-3,4,9,10-tetracarboxy diimide

Chemical Property of N,N'-bis(4-chlorophenyl)-1,7-(disulfuric acid)perylene-3,4,9,10-tetracarboxy diimide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N'-bis(4-chlorophenyl)-1,7-(disulfuric acid)perylene-3,4,9,10-tetracarboxy diimide

There total 2 articles about N,N'-bis(4-chlorophenyl)-1,7-(disulfuric acid)perylene-3,4,9,10-tetracarboxy diimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.6%

3,4,9,10-perylenetetraracarboxylic acid N,N′-di(4-chlorophenyl)diimide (2379-77-3) → N,N'-bis(4-chlorophenyl)-1,7-(disulfuric acid)perylene-3,4,9,10-tetracarboxy diimide (1200827-15-1)

Guidance literature:

With fuming sulphuric acid; at 145 ℃; Inert atmosphere;

DOI:10.1016/j.dyepig.2018.12.002

Reference yield:

4-chloro-aniline (106-47-8) + perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride (128-69-8) → N,N'-bis(4-chlorophenyl)-1,7-(disulfuric acid)perylene-3,4,9,10-tetracarboxy diimide (1200827-15-1)

Guidance literature:

Multi-step reaction with 2 steps

1: isoquinoline / 50 - 200 °C / Inert atmosphere

2: fuming sulphuric acid / 145 °C / Inert atmosphere

With isoquinoline; fuming sulphuric acid;

DOI:10.1016/j.dyepig.2018.12.002

upstream raw materials:

3,4,9,10-perylenetetraracarboxylic acid N,N′-di(4-chlorophenyl)diimide

4-chloro-aniline

perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride