(2S,3R,1''S)-3-methyl-4-oxo-4-phenyl-2-[(1''-phenylethyl)-amino]butanoic acid

Base Information

Chemical Name:(2S,3R,1''S)-3-methyl-4-oxo-4-phenyl-2-[(1''-phenylethyl)-amino]butanoic acid
CAS No.:924283-63-6
Molecular Formula:C₁₉H₂₁NO₃
Molecular Weight:311.381
Hs Code.:

Synonyms:(2S,3R,1''S)-3-methyl-4-oxo-4-phenyl-2-[(1''-phenylethyl)-amino]butanoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R,1''S)-3-methyl-4-oxo-4-phenyl-2-[(1''-phenylethyl)-amino]butanoic acid

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Technology Process of (2S,3R,1''S)-3-methyl-4-oxo-4-phenyl-2-[(1''-phenylethyl)-amino]butanoic acid

There total 1 articles about (2S,3R,1''S)-3-methyl-4-oxo-4-phenyl-2-[(1''-phenylethyl)-amino]butanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 2627-86-3
(S)-1-phenyl-ethylamine

: 35504-92-8
(2E)-3-methyl-4-oxo-4-phenylbut-2-enoic acid

: 924283-63-6
(2S,3R,1''S)-3-methyl-4-oxo-4-phenyl-2-[(1''-phenylethyl)-amino]butanoic acid

Guidance literature:: In water; at 40 ℃; for 168h;
DOI:10.1039/b613103d

Reference yield:

: 924283-63-6
(2S,3R,1''S)-3-methyl-4-oxo-4-phenyl-2-[(1''-phenylethyl)-amino]butanoic acid

: 2-amino-3-methyl-4-phenylbutanoic acid

: (2S,3R)-2-amino-3-methyl-4-phenylbutanoic acid

Guidance literature:: With hydrogen bromide; hydrogen; palladium on activated charcoal; In ethanol; water; at 40 ℃; for 24h; under 836.056 Torr;
DOI:10.1039/b613103d

Reference yield:

: 924283-63-6
(2S,3R,1''S)-3-methyl-4-oxo-4-phenyl-2-[(1''-phenylethyl)-amino]butanoic acid

: (2S,3R,4S,1''S)-4-hydroxy-3-methyl-4-phenyl-2-[(1''-phenylethyl)amino]butanoic acid

: 924283-69-2
(2S,3R,4R,1''S)-4-hydroxy-3-methyl-4-phenyl-2-[(1''-phenylethyl)amino]butanoic acid

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 - 5 ℃; for 0.5h; Title compound not separated from byproducts.;
DOI:10.1039/b613103d