N-[1-(4-methoxybenzyl)-1H-indol-3-ylcarbonyl]-N''-4-methoxyphenylthiosemicarbazide

Base Information

Chemical Name:N-[1-(4-methoxybenzyl)-1H-indol-3-ylcarbonyl]-N''-4-methoxyphenylthiosemicarbazide
CAS No.:1396744-16-3
Molecular Formula:C₂₅H₂₄N₄O₃S
Molecular Weight:460.557
Hs Code.:

Synonyms:N-[1-(4-methoxybenzyl)-1H-indol-3-ylcarbonyl]-N''-4-methoxyphenylthiosemicarbazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[1-(4-methoxybenzyl)-1H-indol-3-ylcarbonyl]-N''-4-methoxyphenylthiosemicarbazide

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Technology Process of N-[1-(4-methoxybenzyl)-1H-indol-3-ylcarbonyl]-N''-4-methoxyphenylthiosemicarbazide

There total 5 articles about N-[1-(4-methoxybenzyl)-1H-indol-3-ylcarbonyl]-N''-4-methoxyphenylthiosemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1253113-89-1
1-(4-methoxybenzyl)-1H-indole-3-carbohydrazide

: 2284-20-0
4-Methoxyphenyl isothiocyanate

: 1396744-16-3
N-[1-(4-methoxybenzyl)-1H-indol-3-ylcarbonyl]-N''-4-methoxyphenylthiosemicarbazide

Guidance literature:: In ethanol; for 7h; Inert atmosphere; Reflux;
DOI:10.1002/jhet.864

Reference yield:

: 1402976-44-6
methyl 1-(4-methoxybenzyl)-1H-indole-3-carboxylate

: 1396744-16-3
N-[1-(4-methoxybenzyl)-1H-indol-3-ylcarbonyl]-N''-4-methoxyphenylthiosemicarbazide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / ethylene glycol / 4 h / Inert atmosphere; Reflux

2: ethanol / 7 h / Inert atmosphere; Reflux

With hydrazine hydrate; In ethanol; ethylene glycol;
DOI:10.1002/jhet.864

Reference yield:

: 942-24-5
3-methoxycarbonylindole

: 1396744-16-3
N-[1-(4-methoxybenzyl)-1H-indol-3-ylcarbonyl]-N''-4-methoxyphenylthiosemicarbazide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 8 h / 140 °C / Inert atmosphere

2: hydrazine hydrate / ethylene glycol / 4 h / Inert atmosphere; Reflux

3: ethanol / 7 h / Inert atmosphere; Reflux

With potassium carbonate; hydrazine hydrate; In ethanol; ethylene glycol; N,N-dimethyl-formamide;
DOI:10.1002/jhet.864