Technology Process of C29H38N8O2S2
There total 11 articles about C29H38N8O2S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
4-methyl-[1,2,3]thiadiazole-5-carbonyl chloride; C21H34N4;
With
triethylamine;
In
dichloromethane;
at 0 - 20 ℃;
for 1.25h;
With
sodium hydroxide;
In
dichloromethane; water;
at 20 ℃;
for 0.25h;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: toluene / 20 °C
2.1: ethanol; water / 20 h / 60 °C
3.1: pyrographite / 2 h / 40 °C
3.2: 20 - 50 °C
4.1: hydrogen / palladium 10% on activated carbon
5.1: thiophene; hydrogen / palladium 10% on activated carbon / methanol / 50 °C
6.1: hydrogen / palladium 10% on activated carbon / methanol
7.1: potassium hydroxide / isopropyl alcohol / 18 h / Heating / reflux
8.1: triethylamine / dichloromethane / 1.25 h / 0 - 20 °C
8.2: 0.25 h / 20 °C
With
thiophene; potassium hydroxide; hydrogen; pyrographite; triethylamine;
palladium 10% on activated carbon;
In
methanol; ethanol; dichloromethane; water; isopropyl alcohol; toluene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hydrogen / palladium 10% on activated carbon
2.1: thiophene; hydrogen / palladium 10% on activated carbon / methanol / 50 °C
3.1: hydrogen / palladium 10% on activated carbon / methanol
4.1: potassium hydroxide / isopropyl alcohol / 18 h / Heating / reflux
5.1: triethylamine / dichloromethane / 1.25 h / 0 - 20 °C
5.2: 0.25 h / 20 °C
With
thiophene; potassium hydroxide; hydrogen; triethylamine;
palladium 10% on activated carbon;
In
methanol; dichloromethane; isopropyl alcohol;