N-[2-((5Z,10Z,14Z,19Z)-20-[2-(2,2-Dimethyl-propionylamino)-phenyl]-10,15-bis-{2-[2-(2,5,6-trimethyl-benzoimidazol-1-yl)-acetylamino]-phenyl}-porphyrin-5-yl)-phenyl]-2,2-dimethyl-propionamide

Base Information

Chemical Name:N-[2-((5Z,10Z,14Z,19Z)-20-[2-(2,2-Dimethyl-propionylamino)-phenyl]-10,15-bis-{2-[2-(2,5,6-trimethyl-benzoimidazol-1-yl)-acetylamino]-phenyl}-porphyrin-5-yl)-phenyl]-2,2-dimethyl-propionamide
CAS No.:104089-94-3
Molecular Formula:C₇₈H₇₄N₁₂O₄
Molecular Weight:1243.52
Hs Code.:

N-[2-((5Z,10Z,14Z,19Z)-20-[2-(2,2-Dimethyl-propionylamino)-phenyl]-10,15-bis-{2-[2-(2,5,6-trimethyl-benzoimidazol-1-yl)-acetylamino]-phenyl}-porphyrin-5-yl)-phenyl]-2,2-dimethyl-propionamide

Synonyms:N-[2-((5Z,10Z,14Z,19Z)-20-[2-(2,2-Dimethyl-propionylamino)-phenyl]-10,15-bis-{2-[2-(2,5,6-trimethyl-benzoimidazol-1-yl)-acetylamino]-phenyl}-porphyrin-5-yl)-phenyl]-2,2-dimethyl-propionamide

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Chemical Property of N-[2-((5Z,10Z,14Z,19Z)-20-[2-(2,2-Dimethyl-propionylamino)-phenyl]-10,15-bis-{2-[2-(2,5,6-trimethyl-benzoimidazol-1-yl)-acetylamino]-phenyl}-porphyrin-5-yl)-phenyl]-2,2-dimethyl-propionamide

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Technology Process of N-[2-((5Z,10Z,14Z,19Z)-20-[2-(2,2-Dimethyl-propionylamino)-phenyl]-10,15-bis-{2-[2-(2,5,6-trimethyl-benzoimidazol-1-yl)-acetylamino]-phenyl}-porphyrin-5-yl)-phenyl]-2,2-dimethyl-propionamide

There total 7 articles about N-[2-((5Z,10Z,14Z,19Z)-20-[2-(2,2-Dimethyl-propionylamino)-phenyl]-10,15-bis-{2-[2-(2,5,6-trimethyl-benzoimidazol-1-yl)-acetylamino]-phenyl}-porphyrin-5-yl)-phenyl]-2,2-dimethyl-propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3363-56-2
2,5,6-trimethylbenzimidazole

: 104089-94-3
N-[2-((5Z,10Z,14Z,19Z)-20-[2-(2,2-Dimethyl-propionylamino)-phenyl]-10,15-bis-{2-[2-(2,5,6-trimethyl-benzoimidazol-1-yl)-acetylamino]-phenyl}-porphyrin-5-yl)-phenyl]-2,2-dimethyl-propionamide

Guidance literature:: Multi-step reaction with 4 steps

1: 46 percent / 1.) sodium hydride / tetrahydrofuran / 1.) 3 h; 2.) 1 h, reflux

2: 73 percent / 48 percent HBr / H₂O / 2 h / Heating

3: thionyl chloride / CH₂Cl₂; dimethylformamide / Ambient temperature

4: 1.) pyridine; 2.) pyridine / 1.) dichloromethane, 2 h; 2.) dichloromethane, 0 deg C

With pyridine; thionyl chloride; hydrogen bromide; sodium hydride; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja00282a020

Reference yield:

: 104070-09-9
methyl 2-acetate

: 104089-94-3
N-[2-((5Z,10Z,14Z,19Z)-20-[2-(2,2-Dimethyl-propionylamino)-phenyl]-10,15-bis-{2-[2-(2,5,6-trimethyl-benzoimidazol-1-yl)-acetylamino]-phenyl}-porphyrin-5-yl)-phenyl]-2,2-dimethyl-propionamide

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / 48 percent HBr / H₂O / 2 h / Heating

2: thionyl chloride / CH₂Cl₂; dimethylformamide / Ambient temperature

3: 1.) pyridine; 2.) pyridine / 1.) dichloromethane, 2 h; 2.) dichloromethane, 0 deg C

With pyridine; thionyl chloride; hydrogen bromide; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja00282a020

Reference yield:

: 104070-10-2
hydrobromide salt of 2-acetic acid

: 104089-94-3
N-[2-((5Z,10Z,14Z,19Z)-20-[2-(2,2-Dimethyl-propionylamino)-phenyl]-10,15-bis-{2-[2-(2,5,6-trimethyl-benzoimidazol-1-yl)-acetylamino]-phenyl}-porphyrin-5-yl)-phenyl]-2,2-dimethyl-propionamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / CH₂Cl₂; dimethylformamide / Ambient temperature

2: 1.) pyridine; 2.) pyridine / 1.) dichloromethane, 2 h; 2.) dichloromethane, 0 deg C

With pyridine; thionyl chloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja00282a020