O-Benzyl-N²,N⁵-dibenzoyl-2,5-diamino-4-(1-(methoxycarbonyl)-2-oxopropyl)phenol

Base Information

Chemical Name:O-Benzyl-N²,N⁵-dibenzoyl-2,5-diamino-4-(1-(methoxycarbonyl)-2-oxopropyl)phenol
CAS No.:124400-61-9
Molecular Formula:C₃₂H₂₈N₂O₆
Molecular Weight:536.584
Hs Code.:

O-Benzyl-N<sup>2</sup>,N<sup>5</sup>-dibenzoyl-2,5-diamino-4-(1-(methoxycarbonyl)-2-oxopropyl)phenol

Synonyms:O-Benzyl-N²,N⁵-dibenzoyl-2,5-diamino-4-(1-(methoxycarbonyl)-2-oxopropyl)phenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-Benzyl-N²,N⁵-dibenzoyl-2,5-diamino-4-(1-(methoxycarbonyl)-2-oxopropyl)phenol

Chemical Property:

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Technology Process of O-Benzyl-N²,N⁵-dibenzoyl-2,5-diamino-4-(1-(methoxycarbonyl)-2-oxopropyl)phenol

There total 1 articles about O-Benzyl-N²,N⁵-dibenzoyl-2,5-diamino-4-(1-(methoxycarbonyl)-2-oxopropyl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 114996-60-0
N¹,N⁴-Dibenzoyl-2-(benzyloxy)-p-benzoquinone Diimine

: 105-45-3
acetoacetic acid methyl ester

: 124400-61-9
O-Benzyl-N²,N⁵-dibenzoyl-2,5-diamino-4-(1-(methoxycarbonyl)-2-oxopropyl)phenol

: O-Benzyl-N²,N⁵-dibenzoyl-2,5-diamino-3-(1-(methoxycarbonyl)-2-oxopropyl)phenol

Guidance literature:: With sodium methylate; In tetrahydrofuran; Yields of byproduct given; 1) THF, -78 deg C, 4 h, 2) 0 deg C, 8 h;
DOI:10.1021/jo00291a059

Reference yield: 75.0%

: 124400-61-9
O-Benzyl-N²,N⁵-dibenzoyl-2,5-diamino-4-(1-(methoxycarbonyl)-2-oxopropyl)phenol

: 124400-59-5
N⁵,1-Dibenzoyl-5-amino-6-(benzyloxy)-2-methylindole-3-carboxylic Acid Methyl Ester

Guidance literature:: With sulfuric acid; In dichloromethane;
DOI:10.1021/jo00291a059

Reference yield:

: 124400-61-9
O-Benzyl-N²,N⁵-dibenzoyl-2,5-diamino-4-(1-(methoxycarbonyl)-2-oxopropyl)phenol

: 124400-58-4
N⁵,1-Dibenzoyl-N⁵-(phenylsulfonyl)-5-amino-6-(benzyloxy)-2-methylindole-3-carboxylic Acid Methyl Ester

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / H₂SO₄ (20percent in CH₂Cl₂) / CH₂Cl₂

2: 1) KH / 1) THF, 25 deg C, 0.5 h, 2) 25 deg C, 12 h

With sulfuric acid; potassium hydride; In dichloromethane;
DOI:10.1021/jo00291a059