4-(N-(bromoacetyl)amino)phenylarsonous acid

Base Information

• Chemical Name: 4-(N-(bromoacetyl)amino)phenylarsonous acid
• CAS No.: 1070872-42-2
• Molecular Formula: C₈H₉AsBrNO₃
• Molecular Weight: 321.99

Synonyms:4-(N-(bromoacetyl)amino)phenylarsonous acid

Chemical Property of 4-(N-(bromoacetyl)amino)phenylarsonous acid

Chemical Property:

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Technology Process of 4-(N-(bromoacetyl)amino)phenylarsonous acid

There total 2 articles about 4-(N-(bromoacetyl)amino)phenylarsonous acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-(N-(bromoacetyl)amino)phenylarsonic acid (51146-91-9) → 4-(N-(bromoacetyl)amino)phenylarsonous acid (1070872-42-2)

Guidance literature:

With iodine; ascorbic acid; In methanol; at 20 ℃; for 2.5h; Inert atmosphere;

DOI:10.1021/ja110226y

Reference yield:

p-aminophenylarsonic acid (98-50-0) → 4-(N-(bromoacetyl)amino)phenylarsonous acid (1070872-42-2)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium carbonate; potassium hydroxide / dichloromethane; water / 0.25 h / Cooling with ice

2: iodine; ascorbic acid / methanol / 2.5 h / 20 °C / Inert atmosphere

With iodine; sodium carbonate; potassium hydroxide; ascorbic acid; In methanol; dichloromethane; water;

DOI:10.1021/ja110226y

Reference yield: 74.0%

4-(N-(bromoacetyl)amino)phenylarsonous acid (1070872-42-2) + 3,3-dimethyl-D-cysteine (52-67-5) → 4-(N-(S-penicillaminylacetyl)amino)phenylarsenonous acid

Guidance literature:

With methanol; sodium methylate; at 20 ℃; for 0.333333h; Inert atmosphere;

DOI:10.1021/acs.bioconjchem.8b00032

upstream raw materials:

4-(N-(bromoacetyl)amino)phenylarsonic acid

p-aminophenylarsonic acid

Downstream raw materials:

C₃₂H₄₆AsN₇O₁₈S

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