C₂₆H₂₃NO₄

Base Information

Chemical Name:C₂₆H₂₃NO₄
CAS No.:130012-98-5
Molecular Formula:C₂₆H₂₃NO₄
Molecular Weight:413.473
Hs Code.:

C<sub>26</sub>H<sub>23</sub>NO<sub>4</sub>

Synonyms:C₂₆H₂₃NO₄

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Chemical Property of C₂₆H₂₃NO₄

Chemical Property:

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Technology Process of C₂₆H₂₃NO₄

There total 14 articles about C₂₆H₂₃NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1165952-92-0
cyclohexa-1,4-diene

: 130031-64-0,141783-00-8
C₂₆H₁₉NO₃

: 130012-98-5
C₂₆H₂₃NO₄

Guidance literature:: With toluene-4-sulfonic acid; In benzene; at 25 ℃; for 24h;
DOI:10.1021/ja00008a045

Reference yield:

: 62833-92-5
7,8,9,10-tetrahydrophenanthridine

: 130012-98-5
C₂₆H₂₃NO₄

Guidance literature:: Multi-step reaction with 14 steps

1: 78 percent / mCPBA / CH₂Cl₂ / 1 h / 25 °C

2: 87 percent / 20 h / 100 °C

3: 100 percent / K₂CO₃ / methanol / 1 h / 25 °C

4: 92 percent / 2,6-lutidine / CH₂Cl₂ / 1 h / 0 °C

5: 1.) THF, -78 degC to 0 deg C, 2.) -78 deg C to 25 deg C, 1 h

6: 85 percent / mCPBA / CH₂Cl₂ / 2 h / 25 °C

7: 100 percent / Bu₄NF / tetrahydrofuran / 3 h / 42 °C

8: 80 percent / pyridinium chlorochromate, 4-Angstroem molecular sieves / CH₂Cl₂ / 1 h / 25 °C

9: 1.) Pd(CH₃COO)2, Ph₃P, n-BuNH₂, 2.) Cu₂I₂ / 1.) C₆H₆, 25 deg C, 15 min, 2.) 25 deg C, 2 h

10: 1.) AgNO₃, 2.) KCN / 1.) H₂O, C₂H₅OH, THF, 25 deg C, 5 min, 2.) 10 min

11: 59 percent / LDA / toluene; cyclohexane / 1 h / -78 °C

12: 95 percent / 4-(dimethylamino)pyridine / CH₂Cl₂ / 48 h / 25 °C

13: 86 percent / n-Bu₃SnH, AlBN / toluene / 2 h / 80 °C

14: 85 percent / p-toluenesulfonic acid / benzene / 24 h / 25 °C

With 2,6-dimethylpyridine; dmap; potassium cyanide; palladium diacetate; copper (I) iodide; 2,2'-azobis(isobutyronitrile); 4 A molecular sieve; tetrabutyl ammonium fluoride; tri-n-butyl-tin hydride; potassium carbonate; toluene-4-sulfonic acid; silver nitrate; N-butylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; pyridinium chlorochromate; lithium diisopropyl amide; In tetrahydrofuran; methanol; dichloromethane; cyclohexane; toluene; benzene;
DOI:10.1021/ja00008a045

Reference yield:

: 133165-23-8
7,8,9,10-tetrahydrophenanthridine N-oxide

: 130012-98-5
C₂₆H₂₃NO₄

Guidance literature:: Multi-step reaction with 13 steps

1: 87 percent / 20 h / 100 °C

2: 100 percent / K₂CO₃ / methanol / 1 h / 25 °C

3: 92 percent / 2,6-lutidine / CH₂Cl₂ / 1 h / 0 °C

4: 1.) THF, -78 degC to 0 deg C, 2.) -78 deg C to 25 deg C, 1 h

5: 85 percent / mCPBA / CH₂Cl₂ / 2 h / 25 °C

6: 100 percent / Bu₄NF / tetrahydrofuran / 3 h / 42 °C

7: 80 percent / pyridinium chlorochromate, 4-Angstroem molecular sieves / CH₂Cl₂ / 1 h / 25 °C

8: 1.) Pd(CH₃COO)2, Ph₃P, n-BuNH₂, 2.) Cu₂I₂ / 1.) C₆H₆, 25 deg C, 15 min, 2.) 25 deg C, 2 h

9: 1.) AgNO₃, 2.) KCN / 1.) H₂O, C₂H₅OH, THF, 25 deg C, 5 min, 2.) 10 min

10: 59 percent / LDA / toluene; cyclohexane / 1 h / -78 °C

11: 95 percent / 4-(dimethylamino)pyridine / CH₂Cl₂ / 48 h / 25 °C

12: 86 percent / n-Bu₃SnH, AlBN / toluene / 2 h / 80 °C

13: 85 percent / p-toluenesulfonic acid / benzene / 24 h / 25 °C

With 2,6-dimethylpyridine; dmap; potassium cyanide; palladium diacetate; copper (I) iodide; 2,2'-azobis(isobutyronitrile); 4 A molecular sieve; tetrabutyl ammonium fluoride; tri-n-butyl-tin hydride; potassium carbonate; toluene-4-sulfonic acid; silver nitrate; N-butylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; pyridinium chlorochromate; lithium diisopropyl amide; In tetrahydrofuran; methanol; dichloromethane; cyclohexane; toluene; benzene;
DOI:10.1021/ja00008a045